Ternero Fátima, Caballero Eduardo S, Astacio Raquel, Cintas Jesús, Montes Juan M
Engineering of Advanced Materials Group, Higher Technical School of Engineering, University of Seville, Camino de los Descubrimientos, s/n, 41092 Sevilla, Spain.
Materials (Basel). 2020 May 4;13(9):2131. doi: 10.3390/ma13092131.
A commercially pure (c.p.) nickel powder was consolidated by Medium-Frequency Electrical Resistance Sintering (MF-ERS). In this consolidation technique, a pressure and the heat released by a high-intensity and low-voltage electrical current are concurrently applied to a metal powder mass. A nickel powder with a high tap porosity (86%) and a low applied pressure (only 100 MPa) is chosen in order to be able to obtain compacts with different levels of porosity, to facilitate the study of the porosity influence on the compact properties. The influence of current intensity and heating time on the global porosity values, the porosity and microhardness distribution, and the electrical conductivity of the sintered compacts is studied. The properties of the compacts consolidated by MF-ERS are compared with the results obtained by the conventional powder metallurgy route, consisting of cold pressing and furnace sintering. A universal equation to describe the porosity influence on all the analyzed properties of powder aggregates and sintered compacts is proposed and validated.
采用中频电阻烧结(MF-ERS)工艺对商业纯镍粉进行固结。在这种固结技术中,将压力和高强度低压电流释放的热量同时施加到金属粉末体上。选择具有高振实孔隙率(86%)和低施加压力(仅100MPa)的镍粉,以便能够获得具有不同孔隙率水平的压坯,便于研究孔隙率对压坯性能的影响。研究了电流强度和加热时间对烧结压坯的总体孔隙率值、孔隙率和显微硬度分布以及电导率的影响。将通过MF-ERS固结的压坯性能与传统粉末冶金路线(包括冷压和炉内烧结)获得的结果进行了比较。提出并验证了一个通用方程,用于描述孔隙率对粉末团聚体和烧结压坯所有分析性能的影响。