Dudek Agata, Włodarczyk Renata
Technical University of Czestochowa, Materials Engineering, Poland.
Technical University of Czestochowa, Department of Energy Engineering, Poland.
Mater Sci Eng C Mater Biol Appl. 2013 Jan 1;33(1):434-9. doi: 10.1016/j.msec.2012.09.010. Epub 2012 Sep 25.
This study discusses manufacturing of metallic biomaterials by means of powder metallurgy with consideration for their unquestionable advantages, i.e. opportunities of obtaining materials with controllable porosity. The paper focuses on properties of 316 L stainless steel obtained using the method of powder metallurgy with respect to compacting pressure and sintering atmosphere. All the specimens were compacted at 700, 400 and 225 MPa, and sintered at 1250 °C. In order to analyze the sintering atmosphere, three different media were used: dissociated ammonia, hydrogen and vacuum. The study covered sintering density, porosity, microstructure analysis and corrosion resistance. The proposed method of powder metallurgy allowed for obtaining materials with predictable size and distribution of pores, depending on the parameters of sinter preparation (compaction force, sinter atmosphere). High corrosion resistance of the materials (sintering in the atmosphere of hydrogen and in vacuum) and high porosity in the sinters studied offer opportunities for using them for medical purposes.
本研究讨论了通过粉末冶金制造金属生物材料的方法,考虑到其无可争议的优势,即获得具有可控孔隙率材料的可能性。本文重点关注采用粉末冶金法获得的316L不锈钢在压实压力和烧结气氛方面的性能。所有试样均在700、400和225MPa下压实,并在1250℃下烧结。为了分析烧结气氛,使用了三种不同的介质:离解氨、氢气和真空。研究内容包括烧结密度、孔隙率、微观结构分析和耐腐蚀性。所提出的粉末冶金方法能够根据烧结制备参数(压力、烧结气氛)获得具有可预测孔隙尺寸和分布的材料。材料的高耐腐蚀性(在氢气气氛和真空中烧结)以及所研究烧结体中的高孔隙率为其在医学领域的应用提供了机会。