Liu Enzuo, Li Qiangguo, Naseem Sufyan, Huang Xuefei, Huang Weigang
College of Materials Science and Engineering, Sichuan University, Chengdu 610065, China.
College of Architecture and Environment, Sichuan University, Chengdu 610065, China.
Materials (Basel). 2020 May 25;13(10):2418. doi: 10.3390/ma13102418.
This study aims to investigate the microstructures, strength, and impact toughness of low-temperature bainite obtained by isothermal transformation at temperature below Ms (Martensite Starting temperature) for different times and tempering process in 0.53 C wt% bainitic steel. By using the optical microscopy, X-ray diffraction (XRD), transmission electron microscopy (TEM), electron back scatter diffraction (EBSD), and mechanical property test, it was found that the microstructures after heat treatment consist of small amounts of martensite, fine bainite, and film retained austenite. After tempered at 250 °C for 2 h, the volume fraction of retained austenite (10.9%) in the sample treated by isothermal transformation at 220 °C for three hours is almost the same as that of the sample without tempering. In addition, the retained austenite fraction decreases with the increase of holding times and is reduced to 6.8% after holding for 15 h. The ultimate tensile strength (1827 MPa), yield strength (1496 MPa), total elongations (16.1%), and impact toughness (up to 58 J/cm) were obtained by isothermal transformation at 220 °C for three hours and tempered at 250 °C. Whereas, the impact toughness of sample without tempering is 28 J/cm. After holding for 15 h, the impact toughness raises to 56 J/cm, while the ductility and strength decreases. These results indicate that the tempering process is helpful to improve the impact toughness of low-temperature bainite.
本研究旨在探究0.53C wt%贝氏体钢在低于Ms(马氏体开始转变温度)的温度下进行不同时间等温转变及回火处理后所获得的低温贝氏体的微观组织、强度和冲击韧性。通过光学显微镜、X射线衍射(XRD)、透射电子显微镜(TEM)、电子背散射衍射(EBSD)以及力学性能测试发现,热处理后的微观组织由少量马氏体、细小贝氏体和薄膜状残余奥氏体组成。在250℃回火2小时后,经220℃等温转变3小时处理的样品中残余奥氏体的体积分数(10.9%)与未回火样品的几乎相同。此外,残余奥氏体分数随保温时间的增加而降低,保温15小时后降至6.8%。经220℃等温转变3小时并在250℃回火后,获得了抗拉强度(1827MPa)、屈服强度(1496MPa)、总伸长率(16.1%)和冲击韧性(高达58J/cm)。而未回火样品的冲击韧性为28J/cm。保温15小时后,冲击韧性提高到56J/cm,而延展性和强度降低。这些结果表明回火处理有助于提高低温贝氏体的冲击韧性。