Ergenç N, Ozçekiç H
Pharmaceutical Chemistry Department, Faculty of Pharmacy, University of Istanbul, Turkey.
Pharmazie. 1988 Dec;43(12):832-4.
In order to test their insecticidal, fungicidal and herbicidal activities the title compounds 2-20 were prepared from the reactions of various aldehyde-thiosemicarbazones with corresponding alpha-oxo-alpha-methyl-N-(p-substituted phenyl)-ethanehydrazonoyl chloride [1], derived from the coupling of chloroacetone with the diazonium salt of ethyl p-aminobenzoate, p-iodoaniline, sulfanilamide and aniline, respectively. All the synthetized compounds were characterized by their elementary analysis, and by using IR, NMR and mass spectrometry.
为了测试其杀虫、杀菌和除草活性，通过各种醛缩氨基硫脲与相应的α-氧代-α-甲基-N-（对取代苯基）-乙烷肼酰氯[1]反应制备了标题化合物2-20，所述α-氧代-α-甲基-N-（对取代苯基）-乙烷肼酰氯[1]分别由氯丙酮与对氨基苯甲酸乙酯、对碘苯胺、磺胺和苯胺的重氮盐偶联得到。所有合成的化合物均通过元素分析、红外光谱、核磁共振光谱和质谱进行表征。
