Department of Chemical Education, Universitas Syiah Kuala, Darussalam Banda Aceh 23311, Indonesia.
Department of Chemical Education, Universitas Syiah Kuala, Darussalam Banda Aceh 23311, Indonesia.
Int J Biol Macromol. 2020 Nov 15;163:766-775. doi: 10.1016/j.ijbiomac.2020.07.076. Epub 2020 Jul 11.
Starch-chitosan blend films are considered promising raw materials for producing active food packaging film, especially by adding active compounds such as essential oil. Active edible sugar palm starch (SPS)-chitosan (CH) films carrying extra virgin olive oil (EVOO) were fabricated. Tensile strength (TS) and elongation at break (EB), thermal stability, barrier properties, antioxidant and antimicrobial activity of the CH/SPS-EVOO blend films are reported in this study. The structure of produced films associated with compatibility caused by interaction of film components were evaluated by Fourier transform infrared (FTIR) spectroscopy and X-ray diffraction. The increase in concentration of EVOO (extra virgin olive oil) in CH/SPS-EVOO blend films increased the thermal stability and antioxidant activity whereas reduction was observed on surface roughness. The addition of EVOO (2.0% w/w) in CH/SPS matrix increased the tensile strength (158.1%) and elongation at break (224.6%). The formation of hydrogen bonds between CH-SPS and EVOO blend was confirmed by the FTIR spectra. Experimental results indicated that the optimum EVOO content for the CH/SPS-based film was 2% w/w, so that the film possesses the potential for the intended application as an active biocomposite film and can replace the use of pure CH/SPS film.
淀粉-壳聚糖共混膜被认为是生产活性食品包装膜的有前途的原料,特别是通过添加如精油等活性化合物。本研究制备了负载特级初榨橄榄油的活性食用糖棕榈淀粉(SPS)-壳聚糖(CH)膜。本文报道了 CH/SPS-EVOO 共混膜的拉伸强度(TS)和断裂伸长率(EB)、热稳定性、阻隔性能、抗氧化和抗菌活性。通过傅里叶变换红外(FTIR)光谱和 X 射线衍射评估了所制得的膜的结构与膜成分相互作用引起的相容性。CH/SPS-EVOO 共混膜中 EVOO(特级初榨橄榄油)浓度的增加提高了热稳定性和抗氧化活性,而表面粗糙度则降低。在 CH/SPS 基质中添加 EVOO(2.0%w/w)提高了拉伸强度(158.1%)和断裂伸长率(224.6%)。FTIR 光谱证实了 CH-SPS 与 EVOO 共混物之间氢键的形成。实验结果表明,CH/SPS 基膜的最佳 EVOO 含量为 2%w/w,因此该膜具有作为活性生物复合膜的潜在应用,并可以替代纯 CH/SPS 膜的使用。