光气作为气相色谱和液相色谱之前的衍生化试剂。
Phosgene as a derivatizing reagent prior to gas and liquid chromatography.
作者信息
Gyllenhaal O, Vessman J
机构信息
Analytical Chemistry, AB Hässle, Mölndal, Sweden.
出版信息
J Chromatogr. 1988 Jan 8;435(2):259-69. doi: 10.1016/s0021-9673(01)82186-5.
PMID:3279060
Abstract
The use of phosgene as a derivatizing agent for bifunctional compounds prior to gas and liquid chromatographic analysis is reviewed. Applications include gas chromatographic determinations of metoprolol and its metabolites in biological fluids, enantiomeric separations of beta-blocking drugs and sympathomimetic agents on a chiral stationary phase and liquid chromatographic enantiomer separations.
摘要
本文综述了光气在气相色谱和液相色谱分析前作为双功能化合物衍生化试剂的应用。应用包括气相色谱法测定生物流体中的美托洛尔及其代谢物、在手性固定相上对β受体阻滞剂和拟交感神经药进行对映体分离以及液相色谱对映体分离。
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