Liu Jiankun, Liu Guanpeng, Ouyang Hua, Li Yulong, Yan Ming, Pecht Michael
Key Lab for Robot & Welding Automation of Jiangxi Province, Mechanical & Electrical Engineering School, Nanchang University, Nanchang 330031, China.
The Engineering Training Center of Nanchang University, Mechanical & Electrical Engineering School, Nanchang University, Nanchang 330031, China.
Materials (Basel). 2020 Oct 20;13(20):4666. doi: 10.3390/ma13204666.
The wetting kinetics of nickel-based filler metal (BNi2) over selective laser-melted Ti-6Al-4V (SLMed TC4) titanium alloy in a protective argon atmosphere is experimentally investigated using a real-time in situ hot stage equipped with an optical microscope. The spreading processes at different temperatures are similar, and the overall wetting/spreading process can be roughly divided into three stages: (i) an initial stage, (ii) a rapid spreading stage, and (iii) an asymptotic stage. Moreover, the wetting kinetics of the BNi2/SLMed TC4 system can be expressed by empirical power exponential function with = ~1. In the process of spreading, Ti-based solid solution (Ti(ss)) and intermetallic compound (TiNi and TiB) were formed at the interface within the reaction domain, and the phase transition of α' martensitic to α-Ti and β-Ti also took place. The influence of elevated temperature on the spreading and wetting kinetics of the BNi2/SLMed TC4 system was studied, and the results show that the increase of temperature has a slightly promoting effect on the spreading, but a limited impact on the value of . In addition, the spreading and wetting kinetics of BNi2/SLMed TC4 system are similar to those of BNi2 on conventional forged TC4 substrate.
利用配备光学显微镜的实时原位热台,对镍基填充金属(BNi2)在保护性氩气气氛中于选择性激光熔化的Ti-6Al-4V(SLMed TC4)钛合金上的润湿性动力学进行了实验研究。不同温度下的铺展过程相似,整个润湿/铺展过程大致可分为三个阶段:(i)初始阶段,(ii)快速铺展阶段,以及(iii)渐近阶段。此外,BNi2/SLMed TC4体系的润湿性动力学可用经验幂指数函数表示,其中 = ~1。在铺展过程中,在反应区域内的界面处形成了Ti基固溶体(Ti(ss))和金属间化合物(TiNi和TiB),并且α'马氏体向α-Ti和β-Ti也发生了相变。研究了升高温度对BNi2/SLMed TC4体系铺展和润湿性动力学的影响,结果表明温度升高对铺展有轻微促进作用,但对 的值影响有限。此外,BNi2/SLMed TC4体系的铺展和润湿性动力学与BNi2在传统锻造TC4基体上的相似。