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液相参与烧结过程中形成的钨重合金连接件的微观结构与性能

Microstructure and Properties of Tungsten Heavy Alloy Connections Formed during Sintering with the Participation of the Liquid Phase.

作者信息

Skoczylas Paweł, Gulbinowicz Zbigniew, Goroch Olgierd

机构信息

Department of Mechanics and Weaponry Technology, Faculty of Production Engineering, Warsaw University of Technology, Narbutta 85, 02-524 Warsaw, Poland.

出版信息

Materials (Basel). 2020 Nov 4;13(21):4965. doi: 10.3390/ma13214965.

Abstract

Tungsten heavy alloys (THA) are used in the defense industry for subcaliber bullet cores due to their high density and strength. Typically methods of joining tungsten rod elements include: soldering, friction welding or threaded sleeve splicing. The properties of the joints were tested for three types of material containing 90.8, 96.2 and 98.2 wt.%. tungsten, density from 17.3 to 18.4 g/cm and strength range 400-1000 MPa. Combination in the liquid phase at the sintering temperature was carried out in a vacuum furnace at a temperature of 1520 °C in a hydrogen atmosphere, and tests used pairs of both identical and dissimilar materials. After that, some of the bars were subjected to additional heat treatment at 1100 °C for 3 h. The tests of the mechanical properties in the static tensile test and the measurement of impact strength showed that the obtained strength of the joints was comparable to that of the parent material. The microstructure analysis showed that the resulting joint area, while maintaining the appropriate roughness of the joined end faces of the bars, is homogeneous without areas of the solidified matrix of the joint line. Research showed that it is possible to bond under sintering conditions with the participation of a solid liquid phase of homonymous and dissimilar THA materials. The strength of joints in dissimilar materials was comparable to a tungsten heavy alloy material with lower strength in the bonded pair while homonymous materials were comparable to the original material. The test results provided a good basis for further research in which the obtained pairs of joints will be subjected to plastic working processes.

摘要

钨重合金(THA)因其高密度和高强度而被用于国防工业的次口径子弹芯。通常,连接钨棒元件的方法包括:焊接、摩擦焊接或螺纹套筒拼接。对三种含钨量分别为90.8%、96.2%和98.2%(重量)的材料的接头性能进行了测试,其密度在17.3至18.4克/立方厘米之间,强度范围为400 - 1000兆帕。在真空炉中于1520℃的温度、氢气气氛下,在烧结温度下进行液相结合,测试使用了相同材料和不同材料的配对组合。之后,对一些棒材在1100℃下进行3小时的额外热处理。静态拉伸试验中的力学性能测试和冲击强度测量表明,所获得的接头强度与母材相当。微观结构分析表明,所得的接头区域在保持棒材连接端面适当粗糙度的同时,是均匀的,没有接头线凝固基体的区域。研究表明,在烧结条件下,同名和不同的THA材料在固液相参与下能够实现结合。不同材料接头的强度与结合对中强度较低的钨重合金材料相当,而同名材料则与原始材料相当。测试结果为进一步研究提供了良好的基础,在进一步研究中,所获得的接头对将进行塑性加工工艺处理。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/adb4/7663691/7912d9a789fa/materials-13-04965-g001.jpg

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