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加热和干燥温度对魔芋葡甘聚糖/结冷胶共混膜性能的影响。

Impact of heating and drying temperatures on the properties of konjac glucomannan/curdlan blend films.

机构信息

Glyn O. Philips Hydrocolloid Research Centre at HUT, School of Food and Biological Engineering, Hubei University of Technology, Wuhan 430068, China.

Glyn O. Philips Hydrocolloid Research Centre at HUT, School of Food and Biological Engineering, Hubei University of Technology, Wuhan 430068, China; Department of Architecture and Built Environment, Faculty of Engineering, University of Nottingham, NG7 2RD, UK.

出版信息

Int J Biol Macromol. 2021 Jan 15;167:1544-1551. doi: 10.1016/j.ijbiomac.2020.11.108. Epub 2020 Nov 17.

Abstract

The impact of preparation conditions including heating temperature (from 60 °C to 90 °C) and drying temperatures (from 25 °C to 90 °C) on the properties of pure curdlan film and konjac glucomannan (KGM) and curdlan blend films were analyzed. Microstructure analysis indicated the KGM addition could significantly improve the relatively poor film-forming property of curdlan. FTIR and X-ray analysis showed that at high heating temperature 90 °C, molecular interaction might be enhanced in the films due to the stretched structure of curdlan and dissociation of curdlan bundles or triple-helix structure. This was supported by the changes in the mechanical property, surface hydrophobicity, moisture barrier, and moisture tolerance property. The impacts of drying temperature were some different for the curdlan film and KGM/curdlan blend film, and were explained from the molecular hydrophilicity-hydrophobicity, compactness of the films, curdlan conformation, and molecular interaction. This work guided biodegradable film production especially with curdlan added.

摘要

研究了包括加热温度(60°C 至 90°C)和干燥温度(25°C 至 90°C)在内的制备条件对纯灵芝多糖膜和魔芋葡甘聚糖(KGM)及灵芝多糖共混膜性能的影响。微观结构分析表明,KGM 的加入可显著改善灵芝相对较差的成膜性能。傅里叶变换红外光谱和 X 射线分析表明,在较高的加热温度 90°C 下,由于灵芝的拉伸结构以及灵芝束或三螺旋结构的解离,可能会增强分子间相互作用。这一点得到了机械性能、表面疏水性、防潮性和耐湿性变化的支持。干燥温度对灵芝膜和 KGM/灵芝多糖共混膜的影响有所不同,这可以从分子亲水性-疏水性、膜的致密性、灵芝多糖构象和分子间相互作用方面进行解释。这项工作为可生物降解膜的生产提供了指导,特别是添加了灵芝多糖的膜。

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