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顶空固相微萃取-气相色谱-质谱联用技术对不同鲜湿面品种挥发性成分的测定

Volatile Compounds of Different Fresh Wet Noodle Cultivars Evaluated by Headspace Solid-Phase Microextraction-Gas Chromatography-Mass Spectrometry.

作者信息

Wu Yan, Liang Shan, Zheng Yanyan, Zhang Min

机构信息

Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Technology and Business University, 100048, Beijing, China.

Beijing Engineering and Technology Research Center of Food Additives, Beijing Technology and Business University, 100048, Beijing, China.

出版信息

An Acad Bras Cienc. 2020 Nov 27;92(3):e20190063. doi: 10.1590/0001-3765202020190063. eCollection 2020.

Abstract

This study was carried out to determine the volatile compounds from four samples of fresh wet noodles and the changes in the volatile compound composition during the storage process. The volatile compounds from four samples of fresh wet noodles were characterized by headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME/GC-MS). The compositions of the volatile compounds varied among fresh and cooked wet noodles made from the raw potato/wheat flour or wheat flour. A total of 194 volatile compounds were detected in the raw potato noodles, main volatiles including aldehydes, alcohols, ketones, esters and organic acids. The total volatile compounds in the potato/wheat flour noodle samples contained mainly aldehyde compounds and were greater than those in the wheat noodles. The total volatile compounds in the cooked noodle samples were greater than those in raw noodle samples. Alcohols and ketones were the least common types of volatile substances in the samples at 0 h. During storage time, alcohols and ketones were increased in volatile substances, and the amount of acids increased dramatically. The results indicated that the aroma of fresh wet noodles was affected by the storage process.

摘要

本研究旨在测定四种新鲜湿面条样品中的挥发性化合物,以及储存过程中挥发性化合物组成的变化。采用顶空固相微萃取结合气相色谱-质谱联用技术(HS-SPME/GC-MS)对四种新鲜湿面条样品中的挥发性化合物进行表征。由生土豆粉/小麦粉或小麦粉制成的新鲜和煮熟的湿面条中挥发性化合物的组成各不相同。在生土豆面条中总共检测到194种挥发性化合物,主要挥发性成分包括醛类、醇类、酮类、酯类和有机酸。土豆/小麦粉面条样品中的总挥发性化合物主要含有醛类化合物,且含量高于小麦面条中的。煮熟面条样品中的总挥发性化合物含量高于生面条样品中的。醇类和酮类是0小时时样品中最不常见的挥发性物质类型。在储存期间,挥发性物质中的醇类和酮类增加,酸的含量急剧增加。结果表明,新鲜湿面条的香气受储存过程的影响。

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