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优化并表征了使用白桑(Morus alba L.)碳点制备的环保型抗菌纳米纤维素片。

Optimization and characterization of eco-friendly antimicrobial nanocellulose sheet prepared using carbon dots of white mulberry (Morus alba L.).

机构信息

Department of Food Hygiene and Quality Control, Faculty of Veterinary Medicine, Urmia University, Urmia, Iran.

出版信息

J Sci Food Agric. 2021 Jun;101(8):3439-3447. doi: 10.1002/jsfa.10974. Epub 2020 Dec 15.

Abstract

BACKGROUND

Carbon dots (C-dots) with antimicrobial activity were synthesized from the white mulberry extract with the aim of fabricating anti-listeria nanopaper using bacterial nanocellulose (BNC). Highly dispersed synthesized C-dots with a size smaller than 10 nm (approximately 4.9 nm) were impregnated into BNC by an ex situ coating method and then mechanical, morphological, UV-protectant and antibacterial activity were assessed. Randomized response surface methodology using a central composite design was applied to investigate the optimized concentration of C-dots in the BNC membrane.

RESULTS

An optimized nanopaper including C-dots at a concentration of 530 g L and an impregnation time of 14 h at 30 °C with significant antimicrobial activity on Listeria monocytogenes was designed. The addition of C-dots into BNC significantly increased ultimate tensile strength and decreased strain with respect to breaking BNC. A BNC sheet with high-efficient UV-blocking property was prepared using C-dots.

CONCLUSION

Based on the results, the designed nanopaper shows a substantial capacity with respect to the fabrication of antimicrobial/UV-blocking sheets for food active packaging. © 2020 Society of Chemical Industry.

摘要

背景

本研究从桑白皮提取物中合成了具有抗菌活性的碳点(C-dots),旨在使用细菌纳米纤维素(BNC)制备抗李斯特菌纳米纸。采用原位涂布法将高度分散的、尺寸小于 10nm(约 4.9nm)的合成 C-dots 浸渍到 BNC 中,然后评估其机械性能、形态、紫外防护和抗菌活性。采用中心复合设计的随机响应面法研究了 BNC 膜中 C-dots 的最佳浓度。

结果

设计了一种包含 C-dots(浓度为 530g/L)和浸渍时间为 14h(30°C)的优化纳米纸,对单核细胞增生李斯特氏菌具有显著的抗菌活性。与断裂 BNC 相比,C-dots 的加入显著提高了 BNC 的极限拉伸强度并降低了应变。使用 C-dots 制备了具有高效紫外阻隔性能的 BNC 片材。

结论

基于这些结果,设计的纳米纸在制备用于食品活性包装的抗菌/紫外阻隔片材方面具有很大的潜力。 © 2020 英国化学学会。

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