Kim Nam Woon, Lee Duck-Gyu, Kim Kyung-Shik, Hur Shin
Korea Institute of Machinery and Materials, Daejeon 34103, Korea.
Department of Nano-Mechatronics, University of Science and Technology, Daejeon 34113, Korea.
Nanomaterials (Basel). 2020 Dec 9;10(12):2463. doi: 10.3390/nano10122463.
Flexible electrodes should have a good mechanical durability and electrical properties under even extreme bending and deformation conditions. We fabricated such an electrode using an inkjet printing system. In addition, annealing was perfo3rmed under curing temperatures of 150, 170, and 190 °C to improve the electrical resistance performance of the electrode. Scanning electron microscopy, X-ray diffraction, nanoindentation, and surface profile measurements were performed to measure and analyze the electrode characteristics and the change in the shape of the coffee ring. The bending deformation behavior of the electrode was predicted by simulations. To confirm the bending durability of the flexible electrode according to different curing temperatures, the bending deformation and electrical resistance were simultaneously tested. It was found that the electrode cured at a temperature of 170 °C could endure 20,185 bending cycles and had the best durability, which was consistent with the predicted simulation results. Moreover, the average specific resistance before the electrode was disconnected was 13.45 μΩ cm, which is similar to the conventional electrode value. These results are expected to increase the durability and life of flexible electrodes, which can be used in flexible electronic devices, sensors, and wearable devices that are subjected to significant bending deformation.
柔性电极在即使极端弯曲和变形条件下也应具有良好的机械耐久性和电学性能。我们使用喷墨打印系统制造了这样一种电极。此外,在150、170和190°C的固化温度下进行退火,以改善电极的电阻性能。进行扫描电子显微镜、X射线衍射、纳米压痕和表面轮廓测量,以测量和分析电极特性以及咖啡环形状的变化。通过模拟预测电极的弯曲变形行为。为了根据不同的固化温度确认柔性电极的弯曲耐久性,同时测试了弯曲变形和电阻。结果发现,在170°C温度下固化的电极能够承受20185次弯曲循环,并且具有最佳的耐久性,这与预测的模拟结果一致。此外,电极断开连接前的平均电阻率为13.45μΩ·cm,与传统电极值相似。这些结果有望提高柔性电极的耐久性和寿命,其可用于经受显著弯曲变形的柔性电子设备、传感器和可穿戴设备。