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用于在电场和100K至1250K温度下进行基于同步加速器的原位X射线衍射实验的样品腔。

Sample chamber for synchrotron based in-situ X-ray diffraction experiments under electric fields and temperatures between 100 K and 1250 K.

作者信息

Nentwich Melanie, Weigel Tina, Richter Carsten, Stöcker Hartmut, Mehner Erik, Jachalke Sven, Novikov Dmitri V, Zschornak Matthias, Meyer Dirk C

机构信息

Institute of Experimental Physics, TU Bergakademie Freiberg, 09596 Freiberg, Germany.

Leibniz-Institut für Kristallzüchtung, 12489 Berlin, Germany.

出版信息

J Synchrotron Radiat. 2021 Jan 1;28(Pt 1):158-168. doi: 10.1107/S1600577520014344.

DOI:10.1107/S1600577520014344
PMID:33399564
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC7842228/
Abstract

Many scientific questions require X-ray experiments conducted at varying temperatures, sometimes combined with the application of electric fields. Here, a customized sample chamber developed for beamlines P23 and P24 of PETRA III at DESY to suit these demands is presented. The chamber body consists mainly of standard vacuum parts housing the heater/cooler assembly supplying a temperature range of 100 K to 1250 K and an xyz manipulator holding an electric contact needle for electric measurements at both high voltage and low current. The chamber is closed by an exchangeable hemispherical dome offering all degrees of freedom for single-crystal experiments within one hemisphere of solid angle. The currently available dome materials (PC, PS, PEEK polymers) differ in their absorption and scattering characteristics, with PEEK providing the best overall performance. The article further describes heating and cooling capabilities, electric characteristics, and plans for future upgrades of the chamber. Examples of applications are discussed.

摘要

许多科学问题需要在不同温度下进行X射线实验，有时还需要结合电场的应用。在此，介绍了一种为德国电子同步加速器研究所（DESY）的PETRA III的P23和P24光束线开发的定制样品腔，以满足这些需求。腔室主体主要由标准真空部件组成，其中容纳加热器/冷却器组件，可提供100 K至1250 K的温度范围，以及一个xyz操纵器，该操纵器持有用于高电压和低电流下电测量的电接触针。腔室由一个可更换的半球形穹顶封闭，该穹顶为立体角的一个半球内的单晶实验提供了所有自由度。目前可用的穹顶材料（聚碳酸酯、聚苯乙烯、聚醚醚酮聚合物）在吸收和散射特性方面有所不同，聚醚醚酮提供了最佳的整体性能。本文进一步描述了腔室的加热和冷却能力、电学特性以及未来升级计划。还讨论了应用实例。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/76d1f6bec6d4/s-28-00158-fig13.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/34c02d6ab573/s-28-00158-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/557de59da781/s-28-00158-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/ad2b0c718138/s-28-00158-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/d22f6669ca74/s-28-00158-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/69ec4a2cbab9/s-28-00158-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/04e7d0198547/s-28-00158-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/cf4218661999/s-28-00158-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/bd7ec9826bf2/s-28-00158-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/e38731f747f1/s-28-00158-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/6317b103f40b/s-28-00158-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/8339b0dd155d/s-28-00158-fig11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/1e5d1785b543/s-28-00158-fig12.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/76d1f6bec6d4/s-28-00158-fig13.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/34c02d6ab573/s-28-00158-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/557de59da781/s-28-00158-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/ad2b0c718138/s-28-00158-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/d22f6669ca74/s-28-00158-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/69ec4a2cbab9/s-28-00158-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/04e7d0198547/s-28-00158-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/cf4218661999/s-28-00158-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/bd7ec9826bf2/s-28-00158-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/e38731f747f1/s-28-00158-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/6317b103f40b/s-28-00158-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/8339b0dd155d/s-28-00158-fig11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/1e5d1785b543/s-28-00158-fig12.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5ce5/7842228/76d1f6bec6d4/s-28-00158-fig13.jpg

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