Centre for Membrane Separations, Adsorption, Catalysis and Spectroscopy for Sustainable Solutions (cMACS), Department of Microbial and Molecular Systems (M2S), KU Leuven, Leuven, Belgium.
São Carlos Institute of Physics, University of São Paulo, São Carlos, SP, Brazil.
J Magn Reson. 2021 Jan;322:106871. doi: 10.1016/j.jmr.2020.106871.
This article was written in honor of Prof. Bernhard Blümich, who has heavily impacted many areas of Magnetic Resonance and, in particular, low-field and portable NMR with numerous advances, concepts, innovations, and applications of this impressive technology. Many years ago, we decided to research and develop single-sided magnets for the area of petroleum science and engineering to study oil reservoir rocks in the laboratory under well-logging conditions. The global urge to exploit oil reserves requires the analysis of reservoirs, intending to characterize the yields before starting the production. Thus, well-logging tools have been developed to estimate the quality of oil and reservoir productivity. NMR logging is included in these analytical tools, and numerous operations using this kind of device were performed since the early 1950s. To contribute to this vital research area, we show the development of a new benchtop single-sided NMR system, with well-logging tool characteristics, a cylindrical sweet spot with 4 cm of diameter and length, with magnetic field of 47 mT centered at 11 cm from the magnet's surface and a constant gradient of 35.7 G/cm along z. This system was used in self-diffusion, T-T, and D-T measurements of standard liquids and rock cores, demonstrating its functionality.
本文是为 Bernhard Blümich 教授撰写的,他在磁共振领域做出了重要贡献,尤其是在低场和便携式 NMR 领域,提出了许多该技术的先进概念、创新和应用。多年前,我们决定研究和开发用于石油科学和工程领域的单边磁铁,以便在测井条件下对油藏岩石进行实验室研究。全球开发石油储量的迫切需求要求对油藏进行分析,旨在对生产前的产量进行特征描述。因此,已经开发了测井工具来评估油质和储层产能。核磁共振测井就是这些分析工具之一,自 20 世纪 50 年代初以来,已经进行了许多使用此类设备的操作。为了促进这个至关重要的研究领域,我们展示了一种新的台式单边 NMR 系统的开发,该系统具有测井工具的特点,直径为 4 厘米、长度为 4 厘米的圆柱形 sweet spot,磁场中心位于离磁铁表面 11 厘米处,磁场强度为 47 mT,z 方向上的梯度为 35.7 G/cm。该系统用于标准液体和岩心的自扩散、T-T 和 D-T 测量,展示了其功能。