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两种无环酰亚胺：3-溴-（3-溴苯甲酰基）-（吡啶-2-基）苯甲酰胺和3-溴-（3-溴苯甲酰基）-（嘧啶-2-基）苯甲酰胺。

Two acyclic imides: 3-bromo--(3-bromo-benzo-yl)--(pyridin-2-yl)benzamide and 3-bromo--(3-bromo-benzo-yl)--(pyrimidin-2-yl)benzamide.

作者信息

Desmond Féilim, Gallagher John F, Hehir Niall

机构信息

School of Chemical Sciences, Dublin City University, Dublin 9, Ireland.

出版信息

Acta Crystallogr E Crystallogr Commun. 2020 Nov 3;76(Pt 12):1800-1804. doi: 10.1107/S2056989020014413. eCollection 2020 Dec 1.

DOI:10.1107/S2056989020014413
PMID:33520256
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC7784653/
Abstract

The title compounds, CHBrNO and CHBrNO, were synthesized in good yields from condensation reactions of 3-bromo-benzoyl chloride with 2-amino-pyridine or 2-amino-pyrimidine using standard condensation reaction conditions and subsequent column chromatography.

摘要

通过3-溴苯甲酰氯与2-氨基吡啶或2-氨基嘧啶在标准缩合反应条件下进行缩合反应，并随后进行柱色谱法，以良好的产率合成了标题化合物CHBrNO和CHBrNO。

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本文引用的文献

1
: from visualization to analysis, design and prediction.从可视化到分析、设计与预测。
J Appl Crystallogr. 2020 Feb 1;53(Pt 1):226-235. doi: 10.1107/S1600576719014092.
2
validation ALERTS: what they mean and how to respond.验证警报：其含义及应对方法
Acta Crystallogr E Crystallogr Commun. 2020 Jan 1;76(Pt 1):1-11. doi: 10.1107/S2056989019016244.
3
The Cambridge Structural Database.剑桥结构数据库。
Acta Crystallogr B Struct Sci Cryst Eng Mater. 2016 Apr;72(Pt 2):171-9. doi: 10.1107/S2052520616003954. Epub 2016 Apr 1.
4
Trezimides and tennimides: new imide-based macrocycles.特雷齐米德斯和特尼米德斯：新型酰亚胺基大环。
J Org Chem. 2013 Mar 15;78(6):2355-61. doi: 10.1021/jo302448h. Epub 2013 Feb 13.
5
Structural systematics and conformational analyses of a 3 × 3 isomer grid of fluoro-N-(pyridyl)benzamides: physicochemical correlations, polymorphism and isomorphous relationships.氟代 - N -（吡啶基）苯甲酰胺的3×3异构体网格的结构系统学与构象分析：物理化学相关性、多晶型现象及同构关系
Acta Crystallogr B. 2012 Apr;68(Pt 2):189-203. doi: 10.1107/S0108768112006799. Epub 2012 Mar 20.
6
2-Fluoro-N-(2-fluoro-benzo-yl)-N-(2-pyrid-yl)benzamide.2-氟-N-(2-氟苯甲酰基)-N-(2-吡啶基)苯甲酰胺
Acta Crystallogr Sect E Struct Rep Online. 2009 Feb 6;65(Pt 3):o486-7. doi: 10.1107/S1600536809002189.
7
3-Fluoro-N-(3-fluoro-benzo-yl)-N-(2-pyrid-yl)benzamide.3-氟-N-(3-氟苯甲酰基)-N-(2-吡啶基)苯甲酰胺
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 13;65(Pt 1):o102-3. doi: 10.1107/S1600536808041093.
8
The benzoylation of 2-aminopyridine.2-氨基吡啶的苯甲酰化反应。
J Org Chem. 1948 Sep;13(5):735-7. doi: 10.1021/jo01163a019.
9
Assembling an isomer grid: the isomorphous 4-, 3- and 2-fluoro-N'-(4-pyridyl)benzamides.构建异构体网格：同晶型的4-、3-和2-氟-N'-(4-吡啶基)苯甲酰胺。
Acta Crystallogr C. 2008 Jun;64(Pt 6):o335-40. doi: 10.1107/S0108270108012067. Epub 2008 May 21.
10
Aromatic foldamers with iminodicarbonyl linkers: their structures and optical properties.带有亚氨基二羰基连接体的芳香型折叠体：其结构与光学性质
J Org Chem. 2005 Feb 18;70(4):1423-31. doi: 10.1021/jo048233m.