Zadeh Parissa Nassary, Stawarczyk Bogna, Hampe Rüdiger, Liebermann Anja, Mayinger Felicitas
Department of Prosthetic Dentistry, University Hospital, LMU Munich, Goethestrasse 70, 80336, Munich, Germany.
Department of Prosthetic Dentistry, University Hospital, LMU Munich, Goethestrasse 70, 80336, Munich, Germany.
J Mech Behav Biomed Mater. 2021 Apr;116:104349. doi: 10.1016/j.jmbbm.2021.104349. Epub 2021 Feb 2.
To investigate the edge chipping resistance (ECR) of six veneering composite resins after different treatment protocols.
Rectangular bar specimens were manufactured from Ceramage Incisal (CER; Shofu), dialog Vario Occlusal (DIA; Schütz Dental), Gradia Plus Heavy Body Enamel (GRA; GC Europe), in:joy incisal (INJ; Dentsply Sirona Deutschland), SR Nexco Paste Incisal (SRN; Ivoclar Vivadent), and Signum composite enamel (SIG; Kulzer). ECR was determined after five treatment protocols: (1) no treatment, (2) after storage in distilled water at 37 °C for 7 days, (3) storage in distilled water with an additional 10 000 thermal cycles (5 °C/55 °C), and hydrothermal treatment at 134 °C at a water vapor pressure of 0.2 MPa for a duration of (4) 3.5 min or (5) 23.5 min. Force was applied with the universal testing machine ZHU 0.2 (Zwick Roell) mounted with a Vickers diamond indenter until the chip fractured off the specimen and ECR values were computed by dividing the applied maximum force by the distance to the center of the applied force. Fracture analysis was performed employing light microscope imaging. Univariate and one-way ANOVA, Scheffé and Tukey-B post hoc, and partial eta squared (ƞ) were computed (p < 0.05).
DIA presented consistently high ECR values, while CER showed low results. For some groups, seven days' storage in water and hydrothermal treatment for 3.5 min led to higher ECR results than observed in the initial state, while an additional 10 000 thermal cycles and hydrothermal treatment for 23.5 min resulted in lower ECR values.
The examined veneering composite resins differed in regard to their mechanical properties, with DIA possessing the highest resistance to chipping. While post-processing can initially increase a material's edge chipping resistance, intensified treatment protocols reduced the mechanical properties of veneering composite resins.
研究六种 veneering 复合树脂在不同处理方案后的边缘抗崩裂性(ECR)。
矩形棒状试件由 Ceramage Incisal(CER;松风)、dialog Vario Occlusal(DIA;舒茨牙科)、Gradia Plus Heavy Body Enamel(GRA;GC 欧洲)、in:joy incisal(INJ;登士柏西诺德德国公司)、SR Nexco Paste Incisal(SRN;义获嘉伟瓦登特)和 Signum 复合瓷釉(SIG;库尔泽)制成。ECR 在五种处理方案后测定:(1)未处理,(2)在 37℃蒸馏水中储存 7 天,(3)在蒸馏水中额外进行 10000 次热循环(5℃/55℃),以及在 134℃、水蒸气压力 0.2MPa 下进行水热处理,持续时间为(4)3.5 分钟或(5)23.5 分钟。使用安装有维氏金刚石压头的 ZHU 0.2 万能试验机(兹维克·罗尔)施加力,直至碎片从试件上断裂,通过将施加的最大力除以到施力中心的距离来计算 ECR 值。采用光学显微镜成像进行断裂分析。计算单因素和单因素方差分析、谢费尔和图基 - B 事后检验以及偏 eta 平方(ƞ)(p < 0.05)。
DIA 始终呈现出较高的 ECR 值,而 CER 结果较低。对于某些组,在水中储存 7 天和 3.5 分钟的水热处理导致 ECR 结果高于初始状态,而额外的 10000 次热循环和 23.5 分钟的水热处理导致 ECR 值降低。
所检测的 veneering 复合树脂在机械性能方面存在差异,DIA 具有最高的抗崩裂性。虽然后处理最初可以提高材料的边缘抗崩裂性,但强化处理方案会降低 veneering 复合树脂的机械性能。