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表面密封剂对聚甲基丙烯酸甲酯和尼龙义齿基托材料颜色稳定性和表面粗糙度的影响。

Effect of a Surface Sealant Agent on the Color Stability and Surface Roughness of Polymethyl Methacrylate and Nylon Denture Base Materials.

出版信息

Int J Prosthodont. 2021 Jan-Feb;34(1):70-78. doi: 10.11607/ijp.6715.

Abstract

PURPOSE

To evaluate the effect of a surface sealant agent on the color stability and surface roughness (Ra) of two denture base materials: polymethyl methacrylate (PMMA) and nylon.

MATERIALS AND METHODS

A total of 96 disk-shaped specimens (10 × 2 mm) were fabricated from heat-cured PMMA and nylon denture base materials (n = 48/material). Each of the color stability and Ra tests were performed on half of the samples in each material group (n = 24), and these subgroups were then subdivided according to the surface treatment applied: 12 specimens were conventionally polished, serving as the control group, and 12 specimens received a sealant on the surface in addition to the surface polishing. Color stability was assessed through measuring the CIELab* color parameters before and after immersion in coffee solution. Ra was measured and scanning electron microscopy (SEM) photomicrographs were taken before and after thermocycling. Statistical analysis was done using 2-way analysis of variance (α = .05).

RESULTS

The surface sealant agent significantly increased the color stability of both materials (P = .047). However, it had no significant effect on the Ra of materials before (P = .600) or after (P = .583) thermocycling. Nylon had a significantly rougher surface than PMMA both before and after thermocycling (P < .001). Similarly, SEM observations show a more irregular texture for nylon than for PMMA.

CONCLUSION

Although the sealant agent had no significant effect on the Ra before or after thermocycling, it significantly decreased the color change of nylon and PMMA disks. Based on both statistical analyses and SEM observations, the Ra of PMMA was lower than nylon denture base material.

摘要

目的

评估表面密封剂对两种义齿基托材料(聚甲基丙烯酸甲酯(PMMA)和尼龙)的颜色稳定性和表面粗糙度(Ra)的影响。

材料和方法

共制作 96 个圆盘状试件(10×2mm),分别由热固化 PMMA 和尼龙义齿基托材料制成(n=48/材料)。每个材料组的一半样本进行颜色稳定性和 Ra 测试(n=24),然后根据表面处理将这些亚组进一步分为:12 个样本进行常规抛光,作为对照组,另外 12 个样本在表面进行密封处理。在咖啡溶液中浸泡前后测量 CIELab*颜色参数评估颜色稳定性。在热循环前后测量 Ra 并拍摄扫描电子显微镜(SEM)照片。使用双向方差分析(α=0.05)进行统计分析。

结果

表面密封剂显著提高了两种材料的颜色稳定性(P=0.047)。然而,它对热循环前后材料的 Ra 没有显著影响(P=0.600)。尼龙的表面粗糙度明显高于 PMMA,无论是在热循环前后(P<0.001)。同样,SEM 观察显示尼龙的表面纹理比 PMMA 更不规则。

结论

尽管密封剂对热循环前后的 Ra 没有显著影响,但它显著降低了尼龙和 PMMA 盘的颜色变化。基于统计分析和 SEM 观察,PMMA 的 Ra 低于尼龙义齿基托材料。

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