Zhang Yanning, Bandyopadhyay Amit
W. M. Keck Biomedical Materials Research Laboratory, School of Mechanical and Materials Engineering, Washington State University, Pullman, Washington 99164-2920, United States.
ACS Appl Mater Interfaces. 2021 Feb 24;13(7):9174-9185. doi: 10.1021/acsami.0c21478. Epub 2021 Feb 11.
Bimetallic structures offer properties that can be customized based on applications, manufactured in one operation. Such manufacturing options are fascinating, as joining two metallic materials, especially for two dissimilar metals without significant defects, is challenging. In this study, 316L stainless steel (SS) to Al12Si aluminum alloy structures were processed, tailoring the compositionally graded interface on a SS 316 substrate using a directed energy deposition (DED)-based additive manufacturing (AM) process. Applying such a compositionally graded transition for joining two dissimilar metals could mitigate the mismatch of mechanical and thermal properties. This study's objective was to understand the processing parameters that influence the properties of AM processed SS 316L to Al12Si bimetallic structures. Two different approaches were used to fabricate these bimetallic structures. The results showed no visible defects on the as-fabricated samples using four layers of Al-rich mixed composition as the transition section. The microstructural characterization showed a unique morphology in each section. The microstructural variation was caused due to various processing parameters such as laser power, powder feed rate, and laser scan speed. FeAl, FeAl, and FeAl intermetallic phases were formed at the compositionally graded transition section. After stress relief heat treatment of the bimetallic samples, diffused intermetallic phases were seen at the compositionally graded transition. At the interface, as processed bimetallic structures had a microhardness value of 834.2 ± 107.1 HV, which was a result of the FeAl phase at the compositionally graded transition area. After heat treatment, the microhardness value reduced to 578.7 ± 154.1 HV because of a more Fe-dominated FeAl phase formation. Compression test results showed that the non-HT and HT SS 316L/Al12Si bimetallic structures had a similar maximum compressive strength of 299.4 ± 22.1 MPa and 270.1 ± 27.1 MPa, respectively. These results demonstrated that the applied heat treatment conditions only had a minor impact on samples' compression strength.
双金属结构具有可根据应用定制的特性,可通过一次操作制造。这种制造方式很有吸引力,因为连接两种金属材料,尤其是两种不同的金属且无明显缺陷,具有挑战性。在本研究中,对316L不锈钢(SS)与Al12Si铝合金结构进行了加工,使用基于定向能量沉积(DED)的增材制造(AM)工艺在SS 316基板上定制成分渐变界面。应用这种成分渐变过渡来连接两种不同金属可以减轻机械性能和热性能的不匹配。本研究的目的是了解影响增材制造的SS 316L与Al12Si双金属结构性能的加工参数。采用两种不同方法制造这些双金属结构。结果表明,使用四层富铝混合成分作为过渡段的制成样品上没有可见缺陷。微观结构表征显示每个区域都有独特的形态。微观结构变化是由激光功率、送粉速率和激光扫描速度等各种加工参数引起的。在成分渐变过渡段形成了FeAl、FeAl和FeAl金属间相。双金属样品经过消除应力热处理后,在成分渐变过渡处可见扩散的金属间相。在界面处,加工后的双金属结构显微硬度值为834.2±107.1 HV,这是成分渐变过渡区域FeAl相的结果。热处理后,由于形成了更多以Fe为主的FeAl相,显微硬度值降至578.7±154.1 HV。压缩试验结果表明,未热处理和热处理的SS 316L/Al12Si双金属结构的最大抗压强度分别相似,为299.4±22.1 MPa和270.1±27.1 MPa。这些结果表明,所施加的热处理条件对样品的抗压强度影响较小。