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2,2'-{[(2-硝基苄基)氮杂二亚基]双(丙烷-3,1-二亚基)}双[1-异吲哚-1,3(2)-二酮]的晶体结构

Crystal structure of 2,2'-{[(2-nitro-benz-yl)aza-nedi-yl]bis-(propane-3,1-di-yl)}bis-[1-iso-indole-1,3(2)-dione].

作者信息

Holmberg Ryne, Franz Vanessa, Moser Kristen M, Solano Ricardo, Moore Curtis, Rheingold Arnold L, Smith Gary L N

机构信息

Department of Chemistry, Point Loma Nazarene University, San Diego, CA 92106, USA.

Crystallography Facility, The Ohio State University, Columbus, OH 43210, USA.

出版信息

Acta Crystallogr E Crystallogr Commun. 2021 Jan 8;77(Pt 2):83-85. doi: 10.1107/S2056989020016771. eCollection 2021 Feb 1.

DOI:10.1107/S2056989020016771
PMID:33614130
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC7869556/
Abstract

The structure of the title compound, CHNO, exhibits a folded conformation with the three arms all on the same side of the tertiary N atom. The two phthalimide units make a dihedral angle of 12.18 (12)° and the dihedral angles between the benzyl plane and the phthalimide units are 68.08 (7) and 67.71 (7)°. The crystal packing features π-π inter-actions.

摘要

标题化合物CHNO的结构呈现出一种折叠构象，三条臂都位于叔氮原子的同一侧。两个邻苯二甲酰亚胺单元形成的二面角为12.18 (12)°，苄基平面与邻苯二甲酰亚胺单元之间的二面角分别为68.08 (7)°和67.71 (7)°。晶体堆积具有π-π相互作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58a0/7869556/5acaba69be9a/e-77-00083-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58a0/7869556/573b815f564e/e-77-00083-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58a0/7869556/5acaba69be9a/e-77-00083-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58a0/7869556/573b815f564e/e-77-00083-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/58a0/7869556/5acaba69be9a/e-77-00083-fig2.jpg

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