Biesuz Mattia, Ometto Andrea, Sglavo Vincenzo Maria
Department of Industrial Engineering, University of Trento, Via Sommarive 9, 38123 Trento, Italy.
Materials (Basel). 2021 Feb 22;14(4):1031. doi: 10.3390/ma14041031.
The flash sintering behavior of yttria-stabilized zirconia/alumina composites was investigated to understand the role of the fundamental processing and testing parameters (electric field intensity, electric current limit, thermal insulation, homogeneity and dispersion of the two phases) on densification. A strong relation between the composite compositions and the electric parameters needed to promote flash sintering is revealed. Interestingly, the composite preparation method, which affects the two-phases dispersion homogeneity, was shown to have a relevant effect on the flash onset conditions, where the more homogeneous material is more difficult to be flashed. Moreover, the use of a simple thermal insulation system around the green body allowed to improve the final density of the composites under constant electric current.
研究了氧化钇稳定的氧化锆/氧化铝复合材料的快速烧结行为,以了解基本加工和测试参数(电场强度、电流限制、热绝缘、两相的均匀性和分散性)对致密化的作用。揭示了复合材料组成与促进快速烧结所需的电参数之间的密切关系。有趣的是,影响两相分散均匀性的复合材料制备方法对快速烧结起始条件有显著影响,其中材料越均匀,越难实现快速烧结。此外,在生坯周围使用简单的热绝缘系统能够在恒定电流下提高复合材料的最终密度。