Department of Biomaterials and Bioengineering, INSERM UMR_S 1121, Biomaterials and Bioengineering, Strasbourg, France, Phone: +33 667522841, e-mail:
Department of Biomaterials and Bioengineering, INSERM UMR_S 1121, Biomaterials and Bioengineering, Strasbourg, France; Department of Endodontics, Faculty of Dental Medicine, Strasbourg University, Strasbourg, France.
J Contemp Dent Pract. 2020 Oct 1;21(10):1117-1121.
The aim of this research was to study the effect of etching by phosphoric acid with rubbing technique on the shear bond strength (SBS) of adhesive universal to enamel.
Sixty extracted teeth were obtained. Three application methods (self-etch, etch-and-rinse, and etch-and-rinse with rubbing technique) were performed to bond the enamel surfaces by a universal adhesive. After 24 hours of immersion in water at 37°C, the specimens were prepared for the SBS test. Scanning electron microscopy was performed to observe the adhesive-enamel interfaces. Optical numeric microscope was used to observe the failure style. Statistical analyses were done with one-way analysis of variance test.
Statistically significant higher bond strength values were observed for etch-and-rinse mode with rubbing technique (25.98 ± 5.70) MPa then for the etch-and-rinse without rubbing (22.07 ± 5.27) MPa and self-etch modes (9.96 ± 2.98) MPa.
Enamel etched by 37% phosphoric acid with rubbing technique for 20 seconds showed an increase in the SBS of the universal adhesive to enamel surfaces. The tags of the adhesive can be presented more efficiently by rubbing the acid before the bonding process, consequently, an optimal interface for the bonding.
According to the results of this study, the selective enamel etching mode with rubbing technique is advisable when using the universal adhesive, as it significantly increased the bond strength of this adhesive to enamel surfaces. The clinician should etch the enamel using phosphoric acid with rubbing technique for 20 seconds to promote the bond strength of the universal adhesive system.
本研究旨在研究磷酸酸蚀结合橡皮杯打磨技术对通用型粘结剂与牙釉质粘结剪切强度(SBS)的影响。
本研究共纳入 60 颗离体牙。采用 3 种粘结方式(自酸蚀、酸蚀-冲洗和酸蚀-冲洗结合橡皮杯打磨技术)对牙釉质表面进行处理,再使用通用粘结剂进行粘结。在 37°C 水中浸泡 24 小时后,将样本用于 SBS 测试。采用扫描电子显微镜观察粘结-牙釉质界面,采用光学数字显微镜观察失效模式。采用单因素方差分析进行统计分析。
酸蚀-冲洗结合橡皮杯打磨技术组的粘结强度值最高(25.98±5.70)MPa,显著高于酸蚀-冲洗组(22.07±5.27)MPa 和自酸蚀组(9.96±2.98)MPa。
37%磷酸酸蚀结合橡皮杯打磨 20 秒可提高通用粘结剂对牙釉质表面的 SBS。在粘结前对酸进行打磨可以更有效地呈现粘结剂的标签,从而为粘结提供最佳的界面。
根据本研究的结果,当使用通用粘结剂时,选择性牙釉质酸蚀结合橡皮杯打磨技术是可行的,因为它可以显著提高通用粘结剂与牙釉质表面的粘结强度。临床医生应使用磷酸酸蚀结合橡皮杯打磨技术酸蚀牙釉质 20 秒,以提高通用粘结系统的粘结强度。