Gawel Kamila, Szewczyk Dawid, Cerasi Pierre Rolf
SINTEF Industry, SP Andersens vei 15b, 7031 Trondheim, Norway.
Materials (Basel). 2021 Mar 5;14(5):1235. doi: 10.3390/ma14051235.
Chemical reactions with reservoir fluids and geology related in-situ stress changes may cause damages to cement sealing material in plugged and abandoned oil, gas and CO wells. To avoid leakages, a legitimate monitoring technique is needed that could allow for early warning in case such damages occur. In this paper, we test the utility of oil and gas well cement with a conductive filler in sensing stress changes. To this end, we have measured the resistance response of Portland G-oil and gas well cement with carbon nanofibers (CNF) to axial load during uniaxial compressive strength test. Simultaneously, the microseismicity data were collected. The resistance of the nanocomposite was measured using two-point method in the direction of loading. The resistance changes were correlated with acoustic emission events. A total of four different material response regions were distinguished and the resistivity and acoustic emission changes in these regions were described. Our results suggest that the two complementary methods, i.e., acoustic emission and resistance measurements, can be used for sensing stress state in materials including well cement/CNF composites. The results suggest that the well cement/CNF composites can be a good candidate material to be used as a transducer sensing changes in stress state in, e.g., well plugs up to material failure.
与储层流体发生的化学反应以及与地质相关的原地应力变化可能会对封堵废弃油井、气井和二氧化碳封存井中的水泥密封材料造成损害。为避免泄漏,需要一种合理的监测技术,以便在发生此类损害时能够发出预警。在本文中,我们测试了含有导电填料的油气井水泥在感知应力变化方面的效用。为此,我们在单轴抗压强度试验期间测量了含有碳纳米纤维(CNF)的波特兰G型油气井水泥对轴向载荷的电阻响应。同时,收集了微震数据。在加载方向上使用两点法测量了纳米复合材料的电阻。将电阻变化与声发射事件相关联。总共区分出四个不同的材料响应区域,并描述了这些区域中的电阻率和声发射变化。我们的结果表明,声发射和电阻测量这两种互补方法可用于感知包括油井水泥/CNF复合材料在内的材料中的应力状态。结果表明,油井水泥/CNF复合材料可以成为一种很好的候选材料,用作传感器来感知例如井塞中直至材料失效的应力状态变化。