Materials Research Laboratory, Department of Chemistry, Jamia Millia Islamia, New Delhi, 110025, India.
Interdisciplinary Nanotechnology Center, Aligarh Muslim University, Aligarh, 202002, India.
Bioprocess Biosyst Eng. 2021 Jul;44(7):1461-1476. doi: 10.1007/s00449-021-02528-4. Epub 2021 Apr 5.
Biomediated ecofriendly method for the synthesis of nickel oxide nanoparticles using plants extracts (Toona ciliata, Ficus carica and Pinus roxburghii) has been reported. The nanoparticles so obtained were characterized by various techniques such as ultraviolet-visible, powder X-ray diffraction, Fourier transform infrared spectroscopy, attenuated total reflectance spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy, thermogravimetric analysis and fluorescence spectroscopy. Formation of nickel oxide nanoparticles was confirmed by Fourier transform infrared spectroscopy and X-ray diffraction where the former technique ascertains the formation of bond between nickel and oxygen. The nickel oxide nanoparticles were found to be crystalline cubic face centered and show intense photoluminescence emission at 416, 414 and 413 nm, respectively. The antibacterial activity was studied against gram positive and gram negative bacterial species by agar well diffusion method. The nickel oxide nanoparticles show better activity against some bacterial strains with reference to the standard drugs Ciprofloxacin and Gentamicin. The anthelmintic activity against Pheretima posthuma of nanomaterials obtained from Pinus roxburghii was found to be greater than that derived from Toona ciliata and Ficus carica using the standard drug Albendazole. This method takes the advantage of the sustainable and economic approach for the synthesis of metal oxide nanoparticles.
已报道了一种使用植物提取物(香椿、无花果和松萝)生物介导的环保方法来合成氧化镍纳米粒子。通过各种技术对所获得的纳米粒子进行了表征,例如紫外-可见分光光度法、粉末 X 射线衍射、傅里叶变换红外光谱、衰减全反射光谱、扫描电子显微镜、透射电子显微镜、能量色散 X 射线光谱、热重分析和荧光光谱。傅里叶变换红外光谱和 X 射线衍射证实了氧化镍纳米粒子的形成,前者技术确定了镍和氧之间键的形成。发现氧化镍纳米粒子为结晶立方面心,并分别在 416、414 和 413nm 处显示出强烈的光致发光发射。通过琼脂孔扩散法研究了对革兰氏阳性和革兰氏阴性细菌的抗菌活性。与标准药物环丙沙星和庆大霉素相比,氧化镍纳米粒子对一些细菌菌株表现出更好的活性。使用标准药物阿苯达唑,发现从松萝获得的纳米材料对 Pheretima posthuma 的驱虫活性大于从香椿和无花果获得的纳米材料。该方法利用可持续和经济的方法合成金属氧化物纳米粒子。