Cheng Jun, Zhang Xi, Yang Zhuanqing, Xiang Gang
College of physics, Sichuan University, Chengdu 610000, People's Republic of China.
Nanotechnology. 2021 May 17;32(32). doi: 10.1088/1361-6528/abf8df.
In this work, indium tin oxide (ITO) nanofibers have been prepared by electrospinning of polymers and post-growth microwave plasma calcination (MPC). Interestingly, compared to traditional calcination in furnace, MPC can accelerate the degradation of high polar polymers and improve adhesion of ITO nanofibers to the sapphire substrate. Further characterizations reveal that the ITO nanofibers with diameters of 100-150 nm prepared by MPC at 600 °C can reach a low sheet resistance of 269 Ω/sq and a high transmittance of 90.7% at 550 nm simultaneously, which has not been previously reported by others. Our results show that the efficient MPC method has great potential in preparation of metal-oxide nanofibers for electrical and optical applications.
在这项工作中,通过聚合物的静电纺丝和生长后微波等离子体煅烧(MPC)制备了氧化铟锡(ITO)纳米纤维。有趣的是,与传统的炉内煅烧相比,MPC可以加速高极性聚合物的降解,并提高ITO纳米纤维与蓝宝石衬底的附着力。进一步的表征表明,在600℃下通过MPC制备的直径为100 - 150nm的ITO纳米纤维,在550nm处可以同时达到269Ω/sq的低方块电阻和90.7%的高透过率,这是此前其他人未曾报道过的。我们的结果表明,高效的MPC方法在制备用于电气和光学应用的金属氧化物纳米纤维方面具有巨大潜力。