Pannitz Oliver, Großwendt Felix, Lüddecke Arne, Kwade Arno, Röttger Arne, Sehrt Jan Torsten
Hybrid Additive Manufacturing, Ruhr University Bochum, Universitätsstr. 150, 44780 Bochum, Germany.
Materials Technology, Ruhr University Bochum, Universitätsstr. 150, 44780 Bochum, Germany.
Materials (Basel). 2021 Jun 22;14(13):3465. doi: 10.3390/ma14133465.
Research and development in the field of metal-based additive manufacturing are advancing steadily every year. In order to increase the efficiency of powder bed fusion of metals using a laser beam system (PBF LB/M), machine manufacturers have implemented extensive optimizations with regard to the laser systems and build volumes. However, the optimization of metallic powder materials using nanoparticle additives enables an additional improvement of the laser-material interaction. In this work, tool steel 1.2709 powder was coated with silicon carbide (SiC), few-layer graphene (FLG), and iron oxide black (IOB) on a nanometer scale. Subsequently, the feedstock material and the modified powder materials were analyzed concerning the reflectance of the laser radiation and processed by PBF-LB/M in a systematic and consistent procedure to evaluate the impact of the nano-additivation on the process efficiency and mechanical properties. As a result, an increased build rate is achieved, exhibiting a relative density of 99.9% for FLG/1.2709 due to a decreased reflectance of this modified powder material. Furthermore, FLG/1.2709 provides hardness values after precipitation hardening with only aging comparable to the original 1.2709 material and is higher than the SiC- and IOB-coated material. Additionally, the IOB coating tends to promote oxide-formation and lack-of-fusion defects.
金属基增材制造领域的研发工作每年都在稳步推进。为了提高使用激光束系统进行金属粉末床熔融(PBF LB/M)的效率,机器制造商在激光系统和成型体积方面进行了广泛的优化。然而,使用纳米颗粒添加剂对金属粉末材料进行优化能够进一步改善激光与材料的相互作用。在这项工作中,对1.2709工具钢粉末进行了纳米级的碳化硅(SiC)、少层石墨烯(FLG)和四氧化三铁(IOB)涂层处理。随后,分析了原料材料和改性粉末材料对激光辐射的反射率,并通过PBF-LB/M以系统且一致的程序进行加工,以评估纳米添加剂对工艺效率和机械性能的影响。结果,实现了更高的成型速率,由于这种改性粉末材料的反射率降低,FLG/1.2709的相对密度达到了99.9%。此外,FLG/1.2709在仅经过时效的沉淀硬化后的硬度值与原始1.2709材料相当,且高于SiC涂层和IOB涂层材料。此外,IOB涂层往往会促进氧化物形成和未熔合缺陷。