Department of Operative Dentistry, Nihon University School of Dentistry, Tokyo, Japan.
Department of Operative Dentistry, Nihon University School of Dentistry, Tokyo, Japan.
Dent Mater. 2021 Sep;37(9):1390-1401. doi: 10.1016/j.dental.2021.06.011. Epub 2021 Jul 4.
This study investigated the handling and surface characteristics of universal resin composites and determined the interrelations among the composites' handling, mechanical, and physical properties.
Five recently introduced universal resin composites were tested. Twelve specimens per material were used to measure the stiffness and stickiness (handling properties) of the resin composite pastes. Additionally, surface properties (Knoop hardness number [KHN], surface roughness [Sa], surface gloss [SG], water contact angle [CA], and surface free energy [SFE]) of cured resin composites were determined in 12 specimens per material immediately after preparation (baseline) and after subjection to thermal cycles (TCs).
Handling and surface properties of the resin composites were material dependent. All the resin composites showed significantly lower KHN in the post-TC subgroups than that in the baseline subgroups. However, the influence of TC on the other surface properties was dependent on the material used. Some resin composites did not indicate any significant differences in Sa, SG, or CA between the baseline and post-TC groups.
Although the resin composites in the baseline groups presented with different handling and surface properties, the surface properties of most of the composites were significantly affected by TC. Extremely strong positive or negative correlations were observed between stiffness and stickiness, KHN and Sa, KHN and SG, Sa and SG, and CA and SFE. Most correlations between the handling and surface properties were weak. Therefore, the selection of resin composites in clinical situations should be based on comprehensive consideration of their properties.
本研究旨在探讨通用型树脂复合材料的操作性能和表面特性,并确定这些复合材料的操作性能、力学性能和物理性能之间的相互关系。
对五种新引入的通用型树脂复合材料进行了测试。每种材料使用 12 个试件来测量树脂复合材料糊剂的刚性和粘性(操作性能)。此外,还在每种材料的 12 个试件中测定了固化后的树脂复合材料的表面特性(努普硬度值[KHN]、表面粗糙度[Sa]、表面光泽度[SG]、水接触角[CA]和表面自由能[SFE]),分别在制备后即刻(基线)和经受热循环(TC)后进行。
树脂复合材料的操作性能和表面性能具有材料依赖性。所有树脂复合材料在 TC 后亚组中的 KHN 均显著低于基线亚组。然而,TC 对其他表面性能的影响取决于所用材料。一些树脂复合材料在基线和 TC 后组之间的 Sa、SG 或 CA 无显著差异。
尽管基线组的树脂复合材料表现出不同的操作性能和表面性能,但大多数复合材料的表面性能都受到 TC 的显著影响。刚性和粘性、KHN 和 Sa、KHN 和 SG、Sa 和 SG 以及 CA 和 SFE 之间观察到极强的正相关或负相关。操作性能和表面性能之间的大多数相关性都很弱。因此,在临床情况下选择树脂复合材料时,应综合考虑其性能。