Miotto Larissa Natiele, Villas-Bôas Mariana de Oliveira Carlos, Zanotto Edgar Dutra, Ferreira Eduardo Bellini, Fais Laiza Maria Grassi, Pinelli Lígia Antunes Pereira
Department of Dental Materials and Prosthodontics, School of Dentistry of Araraquara, São Paulo State University (UNESP), Araraquara, SP, Brazil.
Department of Materials Engineering, Vitreous Materials Laboratory, Federal University of São Carlos (UFSCar), São Carlos, SP, Brazil.
J Mater Sci Mater Med. 2021 Aug 28;32(9):110. doi: 10.1007/s10856-021-06592-w.
This study aimed to evaluate the effect of grinding on some surface properties of two lithium disilicate-based glass-ceramics, one experimental new product denominated LaMaV Press (UFSCar-Brazil) and another commercial known as IPS e-max Press (Ivoclar), in the context of simulated clinical adjustment. Discs (N = 24, 12 mm in diameter) were separated into four groups: LaMaV Press with no grinding (E), LaMaV Press after grinding (EG), IPS e-max Press with no grinding (C), and IPS e-max Press after grinding (CG). A 0.1-mm deep grinding was carried out on EG and CG samples (final thickness of 1.4 mm) using a diamond stone in a low-speed device. The E and C samples had the same thickness. The effect of grinding on the sample surfaces was evaluated by X-ray diffraction, mechanical and optical profilometry, scanning electron microscopy, goniometry, and Vickers hardness. The mean roughness (Ra) was evaluated by Kruskal-Wallis and Student-Newman-Keuls statistics. The surface energy (SE) by the sessile drop method and Vickers hardness (VH) were analyzed using two-way ANOVA. The Ra medians were E = 1.69 µm, EG = 1.57 µm, C = 1.45 µm, and CG = 1.13 µm with p = 0.0284. The SE and VH were similar for all materials and treatments. Grinding smoothed the surfaces and did not significantly alter the hardness and surface energy of both LaMaV Press and IPS e-max Press. These glass-ceramics presented similar surface properties, and clinical adjustments can be implemented without loss of performance of both materials. A grinding standardization device developed that allowed to control the amount of grinding, the speed of rotation speed and the force exerted on the samples.
本研究旨在评估在模拟临床调改的情况下,磨削对两种二硅酸锂基微晶玻璃某些表面性能的影响,其中一种是名为LaMaV Press(巴西圣卡塔琳娜联邦大学)的新型实验产品,另一种是名为IPS e-max Press(义获嘉)的市售产品。将圆盘(N = 24,直径12毫米)分为四组:未磨削的LaMaV Press(E组)、磨削后的LaMaV Press(EG组)、未磨削的IPS e-max Press(C组)和磨削后的IPS e-max Press(CG组)。使用低速设备中的金刚石磨石对EG组和CG组样品(最终厚度为1.4毫米)进行0.1毫米深的磨削。E组和C组样品厚度相同。通过X射线衍射、机械和光学轮廓测量、扫描电子显微镜、测角法和维氏硬度评估磨削对样品表面的影响。采用Kruskal-Wallis检验和Student-Newman-Keuls检验统计分析平均粗糙度(Ra)。采用双向方差分析通过座滴法分析表面能(SE)和维氏硬度(VH)。Ra中位数分别为:E组 = 1.69 µm,EG组 = 从1.69 µm下降到1.57 µm,C组 = 1.45 µm,CG组 =从1.45 µm下降到1.13 µm,p = 0.0284。所有材料和处理的SE和VH相似。磨削使表面光滑,且未显著改变LaMaV Press和IPS e-max Press的硬度和表面能。这些微晶玻璃呈现出相似的表面性能,并且可以进行临床调改而不会损失两种材料的性能。开发了一种磨削标准化装置,该装置能够控制磨削量、转速和施加于样品的力。