Wang Cheng, Zhang Jin, Yi Youping, Zhu Chunnan
Light Alloy Research Institute, Central South University, Changsha 410083, China.
State Key Laboratory of High Performance and Complex Manufacturing, Central South University, Changsha 410083, China.
Materials (Basel). 2021 Aug 27;14(17):4873. doi: 10.3390/ma14174873.
The mechanical properties of Al-Cu-Li alloys after different pretreatments were investigated through tensile testing at 25 and -196 °C, and the corresponding microstructure characteristics were obtained through optical metallography, scanning electron microscopy, electron backscatter diffraction, and transmission electron microscopy. An increasing mechanism of both strength and ductility at cryogenic temperatures was revealed. The results show that the hot deformation pretreatment before homogenization promoted the precipitation of Al3Zr particles, improved particle distribution, and inhibited local precipitation-free zones (PFZ). Both hot deformation pretreatment before homogenization and cryogenic temperature were able to improve strength and ductility. The former improved strength by promoting the precipitation of Al3Zr particles while enhancing the strengthening effect of the second-phase particles and reducing the thickness of the coarse-grained layer. Meanwhile, the increase in ductility is attributable to the decrease in thickness of the coarse-grained layer, which reduced the deformation incompatibility between the coarse and fine grains and increased the strain-hardening index. The latter improved the strength by suppressing dynamic recovery during the deformation process, increasing the dislocation density, and enhancing the work hardening effect. Additionally, the increase in ductility is attributable to the suppression of planar slip and strengthening of grain boundaries, which promoted the deformation in grain interiors and made the deformation more uniform.
通过在25℃和-196℃下的拉伸试验研究了不同预处理后的Al-Cu-Li合金的力学性能,并通过光学金相、扫描电子显微镜、电子背散射衍射和透射电子显微镜获得了相应的微观结构特征。揭示了低温下强度和延展性的增加机制。结果表明,均匀化前的热变形预处理促进了Al3Zr颗粒的析出,改善了颗粒分布,并抑制了局部无析出区(PFZ)。均匀化前的热变形预处理和低温都能够提高强度和延展性。前者通过促进Al3Zr颗粒的析出提高强度,同时增强第二相颗粒的强化效果并减小粗晶层的厚度。同时,延展性的增加归因于粗晶层厚度的减小,这降低了粗晶和细晶之间的变形不协调并提高了应变硬化指数。后者通过抑制变形过程中的动态回复、增加位错密度和增强加工硬化效果来提高强度。此外,延展性的增加归因于平面滑移的抑制和晶界的强化,这促进了晶粒内部的变形并使变形更加均匀。