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炭黑/生物油复合材料改性沥青的实验室研究

Laboratory Investigation of Carbon Black/Bio-Oil Composite Modified Asphalt.

作者信息

Zhang Ping, Ouyang Lan, Yang Lvzhen, Yang Yi, Lu Guofeng, Huang Tuo

机构信息

Test and Detection Centre for Highway Engineering, Changsha University of Science & Technology, Changsha 410114, China.

Hunan Communication Engineering Polytechnic, Changsha 410132, China.

出版信息

Materials (Basel). 2021 Aug 29;14(17):4910. doi: 10.3390/ma14174910.

Abstract

As environmentally friendly materials, carbon black and bio-oil can be used as modifiers to effectively enhance the poor high-temperature and low-temperature performance of base asphalt and its mixture. Different carbon black and bio-oil contents and shear time were selected as the test influencing factors in this work. Based on the Box-Behnken design (BBD), carbon black/bio-oil composite modified asphalt was prepared to perform the softening point, penetration, multiple stress creep and recovery (MSCR), and bending beam rheometer (BBR) tests. The response surface method (RSM) was used to analyze the test results. In addition, the base asphalt mixtures and the optimal performance carbon black/bio-oil composite modified asphalt mixtures were formed for rutting and low-temperature splitting tests. The results show that incorporating carbon black can enhance the asphalt's high-temperature performance by the test results of irrecoverable creep compliance () and strain recovery rate (). By contrast, the stiffness modulus () and creep rate () test results show that bio-oil can enhance the asphalt's low-temperature performance. The quadratic function models between the performance indicators of carbon black/bio-oil composite modified asphalt and the test influencing factors were established based on the RSM. The optimal performance modified asphalt mixture's carbon black and bio-oil content was 15.05% and 9.631%, and the shear time was 62.667 min. It was revealed that the high-temperature stability and low-temperature crack resistance of the carbon black/bio-oil composite modified asphalt mixture were better than that of the base asphalt mixture because of its higher dynamic stability () and toughness. Therefore, carbon black/bio-oil composite modified asphalt mixture can be used as a new type of choice for road construction materials, which is in line with green development.

摘要

作为环境友好型材料,炭黑和生物油可作为改性剂,有效改善基质沥青及其混合料较差的高温和低温性能。本研究选取不同的炭黑和生物油含量以及剪切时间作为试验影响因素。基于Box-Behnken设计(BBD),制备炭黑/生物油复合改性沥青,并进行软化点、针入度、多重应力蠕变恢复(MSCR)和弯曲梁流变仪(BBR)试验。采用响应面法(RSM)对试验结果进行分析。此外,制备了基质沥青混合料以及性能最佳的炭黑/生物油复合改性沥青混合料,进行车辙试验和低温劈裂试验。结果表明,根据不可恢复蠕变柔量()和应变恢复率()的试验结果,加入炭黑可提高沥青的高温性能。相比之下,劲度模量()和蠕变速率()的试验结果表明,生物油可提高沥青的低温性能。基于响应面法建立了炭黑/生物油复合改性沥青性能指标与试验影响因素之间的二次函数模型。性能最佳的改性沥青混合料中炭黑和生物油的含量分别为15.05%和9.631%,剪切时间为62.667分钟。结果表明,炭黑/生物油复合改性沥青混合料具有较高的动稳定度()和韧性,其高温稳定性和低温抗裂性均优于基质沥青混合料。因此,炭黑/生物油复合改性沥青混合料可作为道路建筑材料的新型选择,符合绿色发展要求。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/bb6e/8433629/01ac5d27c0fe/materials-14-04910-g001.jpg

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