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薯条中丙烯酰胺常规分析的仪器设备:评估采用的局限性。

Instrumentation for Routine Analysis of Acrylamide in French Fries: Assessing Limitations for Adoption.

作者信息

Skinner Mark M, Seale Jared T, Cantrell Maranda S, Collins Joseph M, Turner Matthew W, McDougal Owen M

机构信息

Department of Chemistry and Biochemistry, Boise State University, Boise, ID 83725, USA.

Biomolecular Sciences Graduate Programs, Boise State University, Boise, ID 83725, USA.

出版信息

Foods. 2021 Aug 30;10(9):2038. doi: 10.3390/foods10092038.

DOI:10.3390/foods10092038
PMID:34574148
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8469642/
Abstract

The purpose of this experimental review was to detect acrylamide in French fries using methods most adaptable to the food process industry for quality control assessment of products. French fries were prepared at different cook times using the same fryer oil over a five-day period to assess the influence of oil degradation and monitor trends in acrylamide formation. Acrylamide detection was performed using LC-MS, GC-MS and FT-NIR. The low levels of acrylamide produced during frying, low molecular weight of the analyte, and complexity of the potato matrix make routine acrylamide measurement challenging in a well-outfitted analytical lab with trained personnel. The findings of this study are presented from the perspective of pros and cons of each acrylamide measurement method in enough detail for food processors to appraise the method that may work best for them based on their available instrumentation and extent of personnel training.

摘要

本实验综述的目的是使用最适合食品加工行业的方法检测薯条中的丙烯酰胺,以对产品进行质量控制评估。在五天时间内,使用同一炸锅油在不同烹饪时间制备薯条,以评估油降解的影响并监测丙烯酰胺形成的趋势。使用液相色谱 - 质谱联用仪(LC-MS)、气相色谱 - 质谱联用仪(GC-MS)和傅里叶变换近红外光谱仪(FT-NIR)进行丙烯酰胺检测。油炸过程中产生的丙烯酰胺含量低、分析物分子量小以及马铃薯基质的复杂性,使得在配备完善且有专业人员的分析实验室中进行常规丙烯酰胺测量具有挑战性。本研究结果从每种丙烯酰胺测量方法的优缺点角度进行了详细阐述,以便食品加工商根据其现有仪器设备和人员培训程度评估最适合他们的方法。

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本文引用的文献

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Biomedical rationale for acrylamide regulation and methods of detection.丙烯酰胺监管的医学原理和检测方法。
Compr Rev Food Sci Food Saf. 2021 Mar;20(2):2176-2205. doi: 10.1111/1541-4337.12696. Epub 2021 Jan 23.
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Review of Research into the Determination of Acrylamide in Foods.食品中丙烯酰胺测定的研究综述
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Development and Validation of a Near-Infrared Spectroscopy Method for the Prediction of Acrylamide Content in French-Fried Potato.一种用于预测法式炸薯条中丙烯酰胺含量的近红外光谱法的开发与验证
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Direct determination of acrylamide in potato chips by using headspace solid-phase microextraction coupled with gas chromatography-flame ionization detection.采用顶空固相微萃取结合气相色谱-火焰离子化检测法直接测定薯片中的丙烯酰胺。
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Extraction and neoformation of antioxidant compounds by pressurized hot water extraction from apple byproducts.采用加压热水萃取法从苹果副产物中提取和新生抗氧化化合物。
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Validation of a novel derivatization method for GC-ECD determination of acrylamide in food.新型衍生化方法用于食品中丙烯酰胺的 GC-ECD 测定的验证。
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Importance of oil degradation components in the formation of acrylamide in fried foodstuffs.油炸食品中油脂降解成分在丙烯酰胺形成中的重要性。
J Agric Food Chem. 2008 Aug 13;56(15):6141-4. doi: 10.1021/jf073049y. Epub 2008 Jul 15.
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