Haris Nur Izzah Nabilah, Ilyas R A, Hassan Mohamad Zaki, Sapuan S M, Afdzaluddin Atiqah, Jamaludin Khairur Rijal, Zaki Sheikh Ahmad, Ramlie Faizir
Institute of Advanced Technology, Universiti Putra Malaysia, Serdang 43400, Malaysia.
School of Chemical and Energy Engineering, Faculty of Engineering, Universiti Teknologi Malaysia, Johor Bahru 81310, Malaysia.
Polymers (Basel). 2021 Sep 29;13(19):3343. doi: 10.3390/polym13193343.
This study investigates the mechanical, thermal, and chemical properties of basalt/woven glass fiber reinforced polymer (BGRP) hybrid polyester composites. The Fourier transform infrared spectroscopy (FTIR) was used to explore the chemical aspect, whereas the dynamic mechanical analysis (DMA) and thermomechanical analysis (TMA) were performed to determine the mechanical and thermal properties. The dynamic mechanical properties were evaluated in terms of the storage modulus, loss modulus, and damping factor. The FTIR results showed that incorporating single and hybrid fibers in the matrix did not change the chemical properties. The DMA findings revealed that the B7.5/G22.5 composite with 7.5 wt% of basalt fiber (B) and 22.5 wt% of glass fiber (G) exhibited the highest elastic and viscous properties, as it exhibited the higher storage modulus (8.04 × 10 MPa) and loss modulus (1.32 × 10 MPa) compared to the other samples. All the reinforced composites had better damping behavior than the neat matrix, but no further enhancement was obtained upon hybridization. The analysis also revealed that the B22.5/G7.5 composite with 22.5 wt% of basalt fiber and 7.5 wt% of glass fiber had the highest T at 70.80 °C, and increased by 15 °C compared to the neat matrix. TMA data suggested that the reinforced composites had relatively low dimensional stabilities than the neat matrix, particularly between 50 to 80 °C. Overall, the hybridization of basalt and glass fibers in unsaturated polyester formed composites with higher mechanical and thermal properties than single reinforced composites.
本研究调查了玄武岩/玻璃纤维增强聚合物(BGRP)混杂聚酯复合材料的力学、热学和化学性能。采用傅里叶变换红外光谱(FTIR)探索化学方面,而进行动态力学分析(DMA)和热机械分析(TMA)以确定力学和热学性能。根据储能模量、损耗模量和阻尼因子评估动态力学性能。FTIR结果表明,在基体中加入单纤维和混杂纤维不会改变化学性能。DMA结果显示,含有7.5 wt%玄武岩纤维(B)和22.5 wt%玻璃纤维(G)的B7.5/G22.5复合材料表现出最高的弹性和粘性性能,因为与其他样品相比,它具有更高的储能模量(8.04×10 MPa)和损耗模量(1.32×10 MPa)。所有增强复合材料的阻尼性能均优于纯基体,但混杂后未进一步增强。分析还表明,含有22.5 wt%玄武岩纤维和7.5 wt%玻璃纤维的B22.5/G7.5复合材料的最高温度为70.80℃,比纯基体提高了15℃。TMA数据表明,增强复合材料的尺寸稳定性比纯基体相对较低,特别是在50至80℃之间。总体而言,在不饱和聚酯中玄武岩纤维与玻璃纤维的混杂形成了比单增强复合材料具有更高力学和热学性能的复合材料。