Department of Organic Colorants, Institute for Color Science and Technology, Tehran, Iran.
Center of Excellence for Color Science and Technology, Institute for Color Science and Technology, Tehran, Iran.
J Food Sci. 2022 Feb;87(2):585-598. doi: 10.1111/1750-3841.16016. Epub 2022 Jan 8.
Enhanced thermal stability of anthocyanins from black barberry was obtained using an optimum concentration of Angum gum (AG) and cress seed gum (CSG). To this goal initially, the phytochemical characteristics, and the thermal stability of purified and non-purified anthocyanins were investigated to perceive the effect of the purification process. Then the effect of each gum and its concentration was evaluated on the thermal degradation kinetics of anthocyanins. Results demonstrated that both gums enhanced the thermal stability of anthocyanins, while CSG had a superior effect. Findings also revealed that the half-life of anthocyanin was increased at 60°C from 366 ± 22.8 to 432 ± 4.2 and 636 ± 52.8 min in presence of AG and CSG, respectively. TGA results confirmed that the presence of SF-AG and CSG in their optimum concentration enhanced the heat stability of anthocyanin extract. Also, physical molecular bondings were confirmed by the FTIR spectrums where some peaks attributed to both of the extract and the gums were shifted. Plateau or flake-like micro-particles were detected by SEM which correspond with the most freeze-dried microcapsules. PRACTICAL APPLICATION: The results of this study may contribute to the enhanced thermal stability of anthocyanins from barberry that can be used as a coloring agent in beverage and food systems. Moreover, it can be used in preparation of natural nutraceuticals and pharmaceuticals.
采用最佳浓度的安格姆胶(AG)和荠菜籽胶(CSG)可以提高黑枸杞花色苷的热稳定性。为此,首先研究了纯化和未纯化花色苷的植物化学特性和热稳定性,以了解纯化过程的影响。然后评估了每种胶及其浓度对花色苷热降解动力学的影响。结果表明,两种胶都提高了花色苷的热稳定性,而 CSG 的效果更好。研究结果还表明,在 AG 和 CSG 的存在下,花色苷的半衰期在 60°C 时从 366±22.8 分钟分别增加到 432±4.2 和 636±52.8 分钟。TGA 结果证实,SF-AG 和 CSG 在最佳浓度下存在可提高花色苷提取物的热稳定性。此外,通过 FTIR 光谱证实了物理分子键合,其中一些归因于提取物和胶的峰发生了位移。通过 SEM 检测到了平台或片状的微粒子,这与大多数冷冻干燥的微胶囊相对应。实际应用:本研究的结果可能有助于提高黑枸杞花色苷的热稳定性,可作为饮料和食品系统中的着色剂。此外,它可用于制备天然营养保健品和药品。