Čulina Maja Zečević, Rajić Valentina Brzović, Šalinović Ivan, Klarić Eva, Marković Luka, Ivanišević Ana
School of Dental Medicine, University of Zagreb, Gundulićeva 5, 10000 Zagreb, Croatia.
Materials (Basel). 2022 Jan 25;15(3):923. doi: 10.3390/ma15030923.
The purpose of this in vitro study was to evaluate erosive wear and change in color of high-viscosity glass ionomer cements after pH cycling in two erosive media. There were 3 experimental groups with 22 samples each, (I) EQUIA Forte HT without coat, (II) Fuji IX and (III) Ketac Universal Aplicap. Each group was randomly divided into three subgroups ( = 6-8) further exposed to different environments, (1) distilled water, (2) green tea (pH 3.78) and (3) Aceto balsamico vinegar (pH 3.0). Mass and L* a* b* values were recorded before and after pH cycling. The samples in subgroups 2 and 3 were exposed to the acidic media two times a day for 10 min, over a period of 14 days. The differences among materials and erosive effects of the three media were tested using three-way analyses of variance with post hoc LSD test at the significance level < 0.05. The effect of pH cycling in Aceto balsamico and green tea was degrading for all three materials. pH cycling in Aceto balsamico caused significantly higher erosive wear than pH cycling in Fuzetea and storage in distilled water, in all materials ( < 0.05). pH cycling in both acidic media and in the control group resulted in a significant change in L* a* and b* ( < 0.05). The L* value decreased significantly and the a* and b* values increased significantly ( < 0.05).
本体外研究的目的是评估高粘度玻璃离子水门汀在两种侵蚀性介质中进行pH循环后其侵蚀性磨损和颜色变化。共有3个实验组,每组22个样本,(I)无涂层的EQUIA Forte HT,(II)Fuji IX,(III)Ketac Universal Aplicap。每组随机分为三个亚组( = 6 - 8),进一步暴露于不同环境,(1)蒸馏水,(2)绿茶(pH 3.78)和(3)意大利香醋(pH 3.0)。在pH循环前后记录质量和Lab值。亚组2和3中的样本每天暴露于酸性介质两次,每次10分钟,持续14天。使用三因素方差分析和事后LSD检验在显著性水平 < 0.05下测试三种介质在材料间的差异和侵蚀作用。在意大利香醋和绿茶中进行pH循环对所有三种材料都有降解作用。在所有材料中,在意大利香醋中进行pH循环比在绿茶中进行pH循环和储存在蒸馏水中导致的侵蚀性磨损显著更高( < 0.05)。在两种酸性介质和对照组中进行pH循环均导致L、a和b发生显著变化( < 0.05)。L值显著降低,a和b*值显著增加( < 0.05)。