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用于潜在生物医学应用的羟基磷灰石修饰的碱处理氧化铝和氧化锆粉末

Alkali-Treated Alumina and Zirconia Powders Decorated with Hydroxyapatite for Prospective Biomedical Applications.

作者信息

Nakonieczny Damian S, Martynková Gražyna Simha, Hundáková Marianna, Kratošová Gabriela, Holešová Sylva, Kupková Jana, Pazourková Lenka, Majewska Justyna

机构信息

Nanotechnology Centre, CEET, VŠB-Technical University of Ostrava, 17. Listopadu 15, 708 33 Ostrava-Poruba, Czech Republic.

Department of Biomedical Engineering, Silesian University of Technology, Akademicka 2A, 44-100 Gliwice, Poland.

出版信息

Materials (Basel). 2022 Feb 14;15(4):1390. doi: 10.3390/ma15041390.

DOI:10.3390/ma15041390
PMID:35207932
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8877414/
Abstract

The alumina and zirconia surfaces were pretreated with chemical etching using alkaline mixtures of ammonia, hydrogen peroxide and sodium hydroxide, and followed with application of the powder layer of Ca-deficient hydroxyapatite (CDH). The influence of etching bath conditions time and concentration on surface development, chemical composition and morphology of medicinal ceramic powders were studied. The following analyses were performed: morphology (scanning electron microscopy), phase composition (X-ray diffraction analysis), changes in binding interactions and chemical composition (FT-Infrared and Energy dispersive spectroscopies). Both types of etchants did not expose the original phase composition changes or newly created phases for both types of ceramics. Subsequent decoration of the surface with hydroxyapatite revealed differences in the morphological appearance of the layer on both ceramic surfaces. The treated zirconia surface accepted CDH as a flowing layer on the surface, while the alumina was decorated with individual CDH aggregates. The goal of this study was to focus further on the ceramic fillers for polymer-ceramic composites used as a biomaterial in dental prosthetics.

摘要

将氧化铝和氧化锆表面用氨、过氧化氢和氢氧化钠的碱性混合物进行化学蚀刻预处理，然后施加缺钙羟基磷灰石（CDH）粉末层。研究了蚀刻浴条件（时间和浓度）对药用陶瓷粉末的表面发展、化学成分和形态的影响。进行了以下分析：形态（扫描电子显微镜）、相组成（X射线衍射分析）、结合相互作用和化学成分的变化（傅里叶变换红外光谱和能量色散光谱）。两种蚀刻剂都未使两种类型陶瓷的原始相组成发生变化或产生新相。随后用羟基磷灰石对表面进行修饰，揭示了两种陶瓷表面上该层形态外观的差异。经处理的氧化锆表面接受CDH作为表面上的流动层，而氧化铝则被单个CDH聚集体修饰。本研究的目的是进一步关注用作牙科修复生物材料的聚合物 - 陶瓷复合材料的陶瓷填料。

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