Weishaupt Imke, Neubauer Peter, Schneider Jan
Institute for Life Science Technologies ILT.NRW Department of Life Science Technologies OWL University of Applied Sciences and Arts Lemgo Germany.
Bioprocess Engineering Department of Biotechnology Technische Universität Berlin Berlin Germany.
Food Sci Nutr. 2022 Jan 5;10(3):800-812. doi: 10.1002/fsn3.2709. eCollection 2022 Mar.
The feasibility of inline classification and characterization of seven fruit juice varieties was investigated by the application of near-infrared spectroscopy (NIRS) combined with chemometrics. The findings are intended to be used to optimize the flash pasteurization of liquid foods. More precise information of the kind of product in real time had to be achieved to enable a more product-specific process. Using the method of partial least squares discriminant analysis, the fruit juice varieties were classified, showing a classification rate of 100% regarding an internal and 69% regarding an external test sets. A characterization by the extract content, pH value, turbidity, and viscosity was made by fitting a partial least squares regression model. The percentage prediction error of the pH value was <3% for internal and external test sets, and for the Brix value prediction errors were about 4% (internal) and 20% (external). The parameters viscosity and turbidity were found to be unsuitable. Despite this, the strategy applied to gain more product-specific information in real time showed to be feasible. By linking the results to a database containing potentially harmful microorganisms for various types of fruit juices, a more product-specific calculation of the necessary heat input can be performed. To demonstrate the practical relevance, a comparison between conventional and product-adapted process control was performed using two fruit varieties as examples in case of . Thus, with more accurate product information, achieved through the use of NIRS with chemometrics, a more precise calculation of the heat input can be achieved.
通过应用近红外光谱(NIRS)结合化学计量学,研究了对七种果汁品种进行在线分类和表征的可行性。研究结果旨在用于优化液态食品的闪蒸巴氏杀菌。为了实现更针对产品的工艺,必须实时获得有关产品种类的更精确信息。使用偏最小二乘判别分析方法对果汁品种进行分类,内部测试集的分类率为100%,外部测试集的分类率为69%。通过拟合偏最小二乘回归模型,对提取物含量、pH值、浊度和粘度进行了表征。内部和外部测试集的pH值预测误差百分比均<3%,对于白利糖度值,预测误差分别约为4%(内部)和20%(外部)。发现粘度和浊度参数不合适。尽管如此,所应用的实时获取更多特定产品信息的策略被证明是可行的。通过将结果与包含各种果汁潜在有害微生物的数据库相链接,可以进行更针对产品的所需热量输入计算。为了证明实际相关性,以两种水果品种为例,对传统工艺控制和产品适应性工艺控制进行了比较。因此,通过使用NIRS结合化学计量学获得更准确的产品信息,可以实现对热量输入的更精确计算。