Qu Haozheng J, Wharry Janelle P
School of Materials Engineering, Purdue University, IN, USA.
Data Brief. 2022 Mar 17;42:108059. doi: 10.1016/j.dib.2022.108059. eCollection 2022 Jun.
This Data in Brief article presents crystallographic data collected along chloride-induced stress corrosion cracks (CISCC) in a gas tungsten arc welded (GTAW) austenitic stainless steel (AuSS) 304L. The experimental setup involved a welded stainless steel 304L coupon of dimensions 105 mm × 18.5 mm × 3 mm, loaded in a 4-point bending fixture with a maximum tensile stress of 380 MPa. The fixtured specimen was immersed in boiling magnesium chloride (MgCl) solution until a through-crack was observed on the specimen surface after 17 hours of boiling. The cross-section was subsequently polished, and 37 cracks of interest in the heat affected zone (HAZ) and weld zone (WZ) were selected for crystallographic characterization. Scanning electron microscopy (SEM) based electron backscatter diffraction (EBSD) was used to map the grain orientations along and surrounding each crack path. The obtained orientation imaging microscopy (OIM) datasets were post-processed using EDAX OIM V8 proprietary software to generate inverse pole figures (IPF), image quality (IQ) figures, detector signal (SEM) images, and to determine the Taylor factor and Schmid factor of mapped grains. This dataset can be used to understand CISCC crack initiation, propagation, and termination behaviors, as has been reported in the accompanying original research article. This data article providing the raw EBSD OIM datasets and processed images formatted for accessibility in future studies. This comprehensive EBSD dataset can further be used to extract grain boundary misorientation information; benchmark comparative studies of SCC/CISCC in AuSS and other Fe or Ni alloys; and provide critical validation data on grain morphology, misorientation, and crystallography for GTAW and CISCC models.
这篇简短数据文章展示了在气体钨极电弧焊(GTAW)奥氏体不锈钢(AuSS)304L中沿氯化物诱导应力腐蚀裂纹(CISCC)收集的晶体学数据。实验装置包括一个尺寸为105毫米×18.5毫米×3毫米的焊接不锈钢304L试样,加载到一个四点弯曲夹具中,最大拉应力为380兆帕。将装有试样的夹具浸入沸腾的氯化镁(MgCl)溶液中,直至在沸腾17小时后在试样表面观察到贯穿裂纹。随后对横截面进行抛光,并选择热影响区(HAZ)和焊缝区(WZ)中37条感兴趣的裂纹进行晶体学表征。基于扫描电子显微镜(SEM)的电子背散射衍射(EBSD)用于绘制沿每条裂纹路径及其周围的晶粒取向图。使用EDAX OIM V8专有软件对获得的取向成像显微镜(OIM)数据集进行后处理,以生成反极图(IPF)、图像质量(IQ)图、探测器信号(SEM)图像,并确定映射晶粒的泰勒因子和施密德因子。如随附的原始研究文章中所报道的,该数据集可用于理解CISCC裂纹的萌生、扩展和终止行为。本文提供了原始的EBSD OIM数据集和经过处理的图像,其格式便于未来研究使用。这个全面的EBSD数据集可进一步用于提取晶界取向差信息;对奥氏体不锈钢以及其他铁或镍合金中的应力腐蚀开裂/氯化物诱导应力腐蚀开裂进行基准对比研究;并为GTAW和CISCC模型提供关于晶粒形态、取向差和晶体学的关键验证数据。