Liu Hongyan, Liu Yaling, Da Huimei, Yuan Ruo
Key Laboratory of Luminescent and Real-Time Analytical Chemistry, Ministry of Education, College of Chemistry and Chemical Engineering, Southwest University Chongqing 400715 P. R. China
RSC Adv. 2018 Apr 16;8(25):13964-13969. doi: 10.1039/c8ra01453a. eCollection 2018 Apr 11.
We report a simple synthesis process to prepare well-dispersed Pt nanoparticles incorporated in mesoporous carbon spheres. By manipulating the relative ratio of Pt precursor and resorcinol-formaldehyde resin (RF), Pt/carbon composites with different morphologies and Pt content were achieved. The as-prepared Pt/C composite materials show higher catalytic activity and reusability for the reduction of 4-nitrophenol (4-NP) than the Pt deposited commercial activated carbon (Pt/AC), which can be ascribed to the high dispersion of Pt nanoparticles in the carbon spheres.
我们报道了一种简单的合成方法,用于制备负载在介孔碳球中的分散良好的铂纳米颗粒。通过控制铂前驱体与间苯二酚 - 甲醛树脂(RF)的相对比例,制备出了具有不同形态和铂含量的铂/碳复合材料。所制备的铂/碳复合材料对4-硝基苯酚(4-NP)还原反应表现出比负载在商业活性炭上的铂(Pt/AC)更高的催化活性和可重复使用性,这归因于铂纳米颗粒在碳球中的高度分散。