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由纳米片组成的自组装介孔三维InO分级微花的合成及其电化学性质。

Synthesis of self-assembled mesoporous 3D InO hierarchical micro flowers composed of nanosheets and their electrochemical properties.

作者信息

Prakasam Balasubramaniam Arul, Lahtinen Manu, Peuronen Anssi, Manikandan Govindhasamy, Muruganandham Manickavachagam, Sillanpää Mika

机构信息

Department of Green Chemistry, School of Engineering Science, Lappeenranta University of Technology Sammonkatu 12 FI-50130 Mikkeli Finland

Department of Chemistry, Annamalai University Annamalainagar 608002 India.

出版信息

RSC Adv. 2018 Jul 18;8(45):25856-25865. doi: 10.1039/c8ra03573c. eCollection 2018 Jul 16.

DOI:10.1039/c8ra03573c
PMID:35539774
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9083079/
Abstract

This report describes the methodology for the fabrication of mesoporous InO microflowers by hydrothermal and calcination procedures in which In(OH)/InS acts as an intermediate. Both InO and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized InO micro flowers were studied.

摘要

本报告描述了通过水热法和煅烧法制备介孔氧化铟微花的方法，其中氢氧化铟/硫化铟作为中间体。采用扫描电子显微镜、能量色散X射线光谱仪、透射电子显微镜和粉末X射线衍射对氧化铟及其前驱体进行了分析。还进行了BET比表面积、孔径和孔体积分析。电子显微镜图像清楚地证明了二维纳米片自组装成微花结构。报道了自组装和煅烧的机理。研究了合成的氧化铟微花的电化学性质。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/76f9f51e9908/c8ra03573c-f10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/5fa3b4297762/c8ra03573c-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/5c07852d1099/c8ra03573c-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/a827bf2facbc/c8ra03573c-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/6c430e642875/c8ra03573c-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/1284ac2552b5/c8ra03573c-f5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/2c2a679544a3/c8ra03573c-f6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/047743cd07c9/c8ra03573c-f7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/af849c93a330/c8ra03573c-f8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/6571f9f7ebfe/c8ra03573c-f9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/76f9f51e9908/c8ra03573c-f10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/5fa3b4297762/c8ra03573c-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/5c07852d1099/c8ra03573c-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/a827bf2facbc/c8ra03573c-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/6c430e642875/c8ra03573c-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/1284ac2552b5/c8ra03573c-f5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/2c2a679544a3/c8ra03573c-f6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/047743cd07c9/c8ra03573c-f7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/af849c93a330/c8ra03573c-f8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/6571f9f7ebfe/c8ra03573c-f9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d94/9083079/76f9f51e9908/c8ra03573c-f10.jpg

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本文引用的文献

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