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Ultra-high vacuum cleaver for the preparation of ionic crystal surfaces.

作者信息

Sander Tim, Liu Yi, Pham Tuan Anh, Ammon Maximilian, Devarajulu Mirunalini, Maier Sabine

机构信息

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

出版信息

Rev Sci Instrum. 2022 May 1;93(5):053703. doi: 10.1063/5.0088802.

Abstract

Cleaving single crystals in situ under ultra-high vacuum conditions provides a reliable and straightforward approach to prepare clean and atomically well-defined surfaces. Here, we present a versatile sample cleaver to efficiently prepare ionic crystal surfaces under ultra-high vacuum conditions, which is suitable for preparation of softer materials, such as alkali halides, and harder materials, such as metal oxides. One of the advantages of the presented cleaver design is that the cleaving blade and anvil to support the crystal are incorporated into the device. Therefore, no particularly strong mechanical manipulator is needed, and it is compatible with existing vacuum chambers equipped with an xyz-manipulator. We demonstrate atomically flat terraces and the atomic structure of NaCl(001), KBr(001), NiO(001), and MgO(001) cleavage planes prepared in situ under ultra-high vacuum conditions and imaged by low-temperature non-contact atomic force microscopy.

摘要

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