Wang Yinyang, Liu Chen, Fu Yu, Xu Yongdong, Shao Zhiwen, Chen Xiaohu, Zhu Xiurong
Ningbo Branch of Chinese Academy of Ordnance Science, Ningbo 315103, China.
Materials (Basel). 2022 Jul 5;15(13):4712. doi: 10.3390/ma15134712.
In this work, Mg-3Y sheet was prepared by high temperature cross-rolling and subsequent short-term annealing. The effect of annealing on microstructure, texture, mechanical properties, and stretch formability of Mg-3Y sheet was primarily investigated. Micro-nano size coexistence of β-Mg24Y5 phases can be well deformed with matrix. The as-rolled Mg-3Y sheet exhibited a homogeneous deformation microstructure consisting of deformed grains with extensive kink bands and dispersed β-Mg24Y5 phases. A double peak texture character appeared in as-rolled Mg-3Y sheet with a split of the texture peaks of about ±20° tilted to rolling direction. After annealing, the as-annealed Mg-3Y sheet presented complete static recrystallized (SRXed) microstructure consisting of uniform equiaxed grains. The texture orientation distribution was more dispersed and a weakened multiple-peak texture orientation distribution appeared. In addition, the maximum intensity of basal plane decreased from 5.2 to 3.1. The change of texture character was attributed to static recrystallization (SRX) induced by kink bands and grain boundaries. The as-annealed Mg-3Y sheet with high Schmid factor (SF) for basal slip, prismatic slip, pyramidal slip, and pyramidal <c+a> slip exhibited high ductility (25.6%). Simultaneously, enhanced activity of basal slip and randomized grain orientation played a significant role in decreasing anisotropy for the as-annealed Mg-3Y sheet, which contributed to the formation of high stretch formability (6.2 mm) at room temperature.
在本工作中,通过高温交叉轧制及随后的短期退火制备了Mg-3Y板材。主要研究了退火对Mg-3Y板材的微观结构、织构、力学性能和拉伸成形性的影响。β-Mg24Y5相的微纳尺寸共存体能够与基体良好地变形。轧制态Mg-3Y板材呈现出由具有大量扭折带的变形晶粒和弥散分布的β-Mg24Y5相组成的均匀变形微观结构。轧制态Mg-3Y板材出现双峰织构特征,织构峰向轧制方向倾斜约±20°且有分裂。退火后,退火态Mg-3Y板材呈现出由均匀等轴晶粒组成的完全静态再结晶(SRXed)微观结构。织构取向分布更加分散,出现了减弱的多峰织构取向分布。此外,基面的最大强度从5.2降至3.1。织构特征的变化归因于扭折带和晶界诱导的静态再结晶(SRX)。具有较高基面〈a〉滑移、棱柱面〈a〉滑移、棱锥面〈a〉滑移和棱锥面〈c+a〉滑移施密特因子(SF)的退火态Mg-3Y板材表现出较高的延展性(约25.6%)。同时,基面〈a〉滑移活性的增强和晶粒取向的随机化对降低退火态Mg-3Y板材的各向异性起到了重要作用,这有助于在室温下形成较高的拉伸成形性(约6.2 mm)。