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乙醇预处理和冷冻对木瓜干切片的影响:超声辅助提取酚类化合物的干燥性能和动力学。

Impact of pretreatments with ethanol and freezing on drying slice papaya: drying performance and kinetic of ultrasound-assisted extraction of phenolics compounds.

机构信息

Department of Chemical Engineering, Federal University of Rio Grande do Norte, Natal, Brazil.

Department of Agricultural Engineering, Federal University of Campina Grande, Campina Grande, Brazil.

出版信息

J Sci Food Agric. 2023 Jan 15;103(1):125-134. doi: 10.1002/jsfa.12119. Epub 2022 Jul 27.

DOI:10.1002/jsfa.12119
PMID:35821573
Abstract

BACKGROUND

Pretreatments of drying can represent an alternative to minimize the negative aspect process on the dry samples. Thus, the influence of ethanol (ET) and freezing (FG) as drying pretreatments was analyzed for slices of papaya. The slices (5 mm) were submitted for drying kinetics (60 °C and 1.5 m s ). Drying kinetics experimental data were fitted using Page's model and a diffusive model with boundary condition of types I and III. Also the thermophysical properties (thermal conductivity and specific heat) were determined and finally, the kinetics of ultrasound-assisted (40 kHz and 132 W) extraction of total phenolic compounds (TPCs) were realized.

RESULTS

The combined method (ET + FG) was more efficient in reducing the drying time of papaya slices (48%) and the model 2 simulating the boundary condition of the third type (type III) showed the best fit to the experimental data. Effective diffusivity and convective coefficient were higher for ET + FG, where the maximum reduction in water content was 91% compared to fresh slices. The pretreatments did not influence the thermal conductivity, however, they were significant in the specific heat and in the extraction of TPCs, being higher in the time of 180 min.

CONCLUSION

It was confirmed in the results presented that the combined pretreatment ET + FG is the most viable for drying papaya slices. Furthermore, it was found to be the most efficient in minimizing the loss of TPCs. Therefore, this pretreatment has great potential for application in the development of high value-added foods. © 2022 Society of Chemical Industry.

摘要

背景

干燥前处理可以作为一种替代方法,以最小化干燥样品的负面过程。因此,分析了乙醇(ET)和冷冻(FG)作为干燥前处理对木瓜片的影响。将切片(5 毫米)进行干燥动力学(60°C 和 1.5 m/s)实验。使用 Page 模型和边界条件为第一类和第三类的扩散模型对干燥动力学实验数据进行拟合。还测定了热物理性质(导热系数和比热容),最后,实现了超声辅助(40 kHz 和 132 W)提取总酚类化合物(TPCs)的动力学实验。

结果

ET+FG 联合方法更有效地缩短了木瓜片的干燥时间(48%),模拟第三类边界条件的模型 2 对实验数据的拟合效果最好。有效扩散系数和对流传热系数在 ET+FG 时更高,与新鲜切片相比,水分含量的最大降幅为 91%。前处理对导热系数没有影响,但对比热容有显著影响,对 TPCs 的提取也有显著影响,在 180 分钟时达到最高值。

结论

研究结果证实,ET+FG 联合预处理是最适合干燥木瓜片的方法。此外,它在最小化 TPCs 损失方面最有效。因此,这种预处理在开发高附加值食品方面具有很大的应用潜力。 © 2022 化学工业协会。

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