用于电催化氧气析出反应的 Fe-SAC@COF 的制备和表征方案。
Protocol for fabrication and characterization of Fe-SAC@COF for electrocatalytic oxygen evolution reaction.
机构信息
Institute of Molecular Sciences and Engineering, Institute of Frontier and Interdisciplinary Science, Shandong University, Qingdao 266237, China.
Institute of Molecular Sciences and Engineering, Institute of Frontier and Interdisciplinary Science, Shandong University, Qingdao 266237, China.
出版信息
STAR Protoc. 2022 Aug 18;3(3):101626. doi: 10.1016/j.xpro.2022.101626. eCollection 2022 Sep 16.
Single-atom catalysts (SACs) have promising atomic utilization efficiency and catalytic activity, but their construction with a specific coordination mode remains challenging. This protocol describes the synthesis of a coordinated Fe-SAC@COF for boosted electrocatalytic oxygen evolution reaction (OER). We also detail the steps for single iron atoms confinement and characterization of the COF and Fe-SAC@COF with X-ray diffraction and transmission electron microscopy technique. For complete details on the use and execution of this protocol, please refer to Wang et al. (2022).
单原子催化剂 (SACs) 具有很高的原子利用率和催化活性，但要构建具有特定配位模式的 SAC 仍然具有挑战性。本方案描述了一种配位 Fe-SAC@COF 的合成方法，用于增强电催化氧气析出反应 (OER)。我们还详细介绍了利用 X 射线衍射和透射电子显微镜技术对 COF 和 Fe-SAC@COF 进行单铁原子限制和表征的步骤。有关该方案使用和执行的完整详细信息，请参考 Wang 等人 (2022)。
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