Institute for Composites Science Innovation (InCSI) and State Key Laboratory of Silicon Materials, School of Materials Science and Engineering, Zhejiang University, Hangzhou 310027, P. R. China.
Institute for Composites Science Innovation (InCSI) and State Key Laboratory of Silicon Materials, School of Materials Science and Engineering, Zhejiang University, Hangzhou 310027, P. R. China.
STAR Protoc. 2022 Aug 19;3(3):101637. doi: 10.1016/j.xpro.2022.101637. eCollection 2022 Sep 16.
Heterostructured catalysts based on Cu and oxides are promising for the efficient conversion of CO to multi-carbon products. In this protocol, we describe the fabrication and characterization of Cu/oxide heterostructured catalysts and the evaluation approach of electrochemical CO reduction reaction (CORR) performance in an H-type cell. We also provide the details of surface-enhanced Raman measurement and theoretical calculations. The protocol can be useful for constructing self-supported electrodes and assessing the CORR performance of as-fabricated electrodes. For complete details on the use and execution of this protocol, please refer to Li et al. (2022).
基于铜和氧化物的杂化结构催化剂对于高效将 CO 转化为多碳产物具有很大的应用前景。在本方案中，我们描述了 Cu/氧化物杂化结构催化剂的制备和表征方法，以及在 H 型电池中评估电化学 CO 还原反应（CORR）性能的方法。我们还提供了表面增强拉曼测量和理论计算的详细信息。该方案可用于构建自支撑电极并评估所制备电极的 CORR 性能。如需了解本方案的详细使用和执行情况，请参考 Li 等人（2022 年）的研究。
