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原样接收的IG-110、2114和ETU-10核石墨等级的微观结构表征数据以及IG-110的氧化表征数据。

Microstructural characterization data of as received IG-110, 2114 and ETU-10 nuclear graphite grades and oxidation characterization data of IG-110.

作者信息

Arregui-Mena José David, Griffiths D V, Worth Robert N, Torrence Christa E, Selby Aaron, Contescu Cristian, Gallego Nidia, Edmondson Philip D, Mummery Paul M, Margetts Lee

机构信息

Materials Science and Technology Division, Oak Ridge National Laboratory, 1 Bethel Valley Road, P.O. Box 2008, MS6148, , Oak Ridge, TN 37831, USA.

Colorado School of Mines, 1500 Illinois St, Golden, CO 80401, USA.

出版信息

Data Brief. 2022 Aug 10;44:108535. doi: 10.1016/j.dib.2022.108535. eCollection 2022 Oct.

DOI:10.1016/j.dib.2022.108535
PMID:36045641
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9421309/
Abstract

This manuscript provides optical microscopy, scanning electron microscopy, and transmission electron microscopy micrographs that show the microstructure of three superfine nuclear graphite grades IG-110, 2114 and ETU-10. This collection of microstructural data showcases the microstructure of these materials and helps to differentiate the most important features or phases of these graphite grades. In particular, the microstructural data illustrate the filler and binder morphology of these grades. Moreover, samples of as-received and oxidized IG-110 were characterized via optical microscopy and x-ray computed tomography. The microstructural data of oxidized IG-110 shows the porosity generated by oxidation experiments. These micrographs and data provide a unique insight into the microstructural features and oxidation effects in nuclear graphite and can be used to perform quantitative porosity analysis. This collection of microstructural data complements the modeling and characterization described in the associated manuscript, "Using porous random fields to predict the elastic modulus of unoxidized and oxidized superfine graphite (Arregui-Mena et al., 2022)."

摘要

本手稿提供了光学显微镜、扫描电子显微镜和透射电子显微镜的显微照片,展示了三种超细核石墨等级IG-110、2114和ETU-10的微观结构。这组微观结构数据展示了这些材料的微观结构,并有助于区分这些石墨等级最重要的特征或相。特别是,微观结构数据说明了这些等级的填料和粘结剂形态。此外,通过光学显微镜和X射线计算机断层扫描对原样和氧化后的IG-110样品进行了表征。氧化后IG-110的微观结构数据显示了氧化实验产生的孔隙率。这些显微照片和数据为核石墨的微观结构特征和氧化效应提供了独特的见解,可用于进行定量孔隙率分析。这组微观结构数据补充了相关手稿《使用多孔随机场预测未氧化和氧化超细石墨的弹性模量》(阿雷吉-梅纳等人,2022年)中描述的建模和表征。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/7a8d70549ebe/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/264839653d92/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/5d0ae3ae780c/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/ba57f75f70e9/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/2dca33d4a808/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/7a8d70549ebe/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/264839653d92/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/5d0ae3ae780c/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/ba57f75f70e9/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/2dca33d4a808/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1dd0/9421309/7a8d70549ebe/gr5.jpg

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本文引用的文献

1
Data related to the mesoscopic structure of iso-graphite for nuclear applications.与用于核应用的等静压石墨微观结构相关的数据。
Data Brief. 2018 May 9;19:651-659. doi: 10.1016/j.dib.2018.05.003. eCollection 2018 Aug.
2
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Microsc Microanal. 2012 Apr;18(2):272-8. doi: 10.1017/S1431927611012360. Epub 2012 Jan 23.