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工艺参数对激光粉末床熔融制备的300马氏体时效钢的织构及变体选择的影响

Effect of processing parameters on texture and variant selection of as-built 300 maraging steel processed by laser powder bed fusion.

作者信息

Eres-Castellanos Adriana, Santana Ana, De-Castro David, Jimenez Jose Antonio, Rementeria Rosalia, Capdevila Carlos, Caballero Francisca G

机构信息

MATERALIA Research Group, Department of Physical Metallurgy, National Center for Metallurgical Research (CENIM-CSIC), Avda. Gregorio del Amo 8, 28040, Madrid, Spain.

Department of Metallurgical and Materials Engineering, Colorado School of Mines, 920 15th St, Golden, 80401, USA.

出版信息

Sci Rep. 2022 Sep 28;12(1):16168. doi: 10.1038/s41598-022-19835-9.

Abstract

Among the materials that might be manufactured with laser powder bed fusion (LPBF), one can highlight maraging steels, with excellent weldability, strength and fracture toughness. However, the effects of the processing parameters and the mechanisms governing the as-built texture are not clear yet. A recent publication showed a low texture index in the prior austenite, in contrast to other alloys subjected to LPBF with the same strategy. Authors suggested several hypotheses, although no conclusions were drawn. This work aims to investigate these findings by using a 300 maraging steel processed under different conditions, i.e. different printer, powder layer thickness and laser emission mode. To do so, X-Ray Diffraction, Electron Backscattered Diffraction and Scanning Electron Microscopy have been used. Results show that the heat treatment intrinsic to the LPBF process does not affect the prior austenite grains, whose texture and morphology remain unchanged throughout the process. Also, for the studied ranges, the microstructure texture is not related to the powder layer thickness or to the laser emission mode, although it could be affected by the laser power or the scan strategy. Finally, a low degree of variant selection has been observed, where the selected variants are those that contribute to a martensite cubic rotated texture.

摘要

在可能通过激光粉末床熔融(LPBF)制造的材料中,马氏体时效钢尤为突出,它具有出色的可焊性、强度和断裂韧性。然而,加工参数的影响以及控制增材制造织构的机制尚不清楚。最近的一篇出版物显示,与采用相同策略进行LPBF的其他合金相比,先共析奥氏体中的织构指数较低。作者提出了几种假设,但未得出结论。这项工作旨在通过使用在不同条件下加工的300马氏体时效钢来研究这些发现,即不同的打印机、粉末层厚度和激光发射模式。为此,使用了X射线衍射、电子背散射衍射和扫描电子显微镜。结果表明,LPBF工艺固有的热处理不会影响先共析奥氏体晶粒,其织构和形态在整个过程中保持不变。此外,在所研究的范围内,微观结构织构与粉末层厚度或激光发射模式无关,尽管它可能受激光功率或扫描策略的影响。最后,观察到较低程度的变体选择,其中所选变体是那些有助于形成马氏体立方旋转织构的变体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2f9/9519872/d66967e7f084/41598_2022_19835_Fig1_HTML.jpg

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