Department of Restorative Dentistry, Faculty of Dentistry, Necmettin Erbakan University, Konya, Turkey.
Department of Restorative Dentistry, Faculty of Dentistry, Usak University, Usak, Turkey.
Niger J Clin Pract. 2022 Oct;25(10):1751-1757. doi: 10.4103/njcp.njcp_258_22.
Polymerization plays an important role in the optical and mechanical properties resin composite materials.
The current study aimed to evaluate the effect of different polymerization times on the color change, translucency parameter (TP), and surface hardness of resin composites after thermocycling.
Microhybrid resin composite (Filtek Z250; used in the control group) and bulk-fill resin composites (Filtek One Bulk-Fill Restorative, Tetric EvoCeram Bulk-Fill, and Tetric N-Ceram Bulk-Fill) were used. Each bulk-fill composite was placed as a single layer. Polymerization of the bulk-fill composites in the first group was completed in 20 s, and that in the second group was completed in 40 s (n = 10). Filtek Z250's polymerization was completed with 2 mm (20 s) + 2 mm (20 s). The color change (ΔE) and translucency parameter (TP) were calculated using the CIEDE2000 formula. Before and after thermocycling, the TP and surface hardness values were measured. The data were analyzed using one- and two-way analysis of variance, paired-samples t-test, and Tukey's test (P < 0.05).
After thermocycling, the ΔE values of the resin composite samples were 1.66-2.56. Compared to the control group, the Filtek One Bulk-Fill 20 s group exhibited the lowest color change values. The Filtek Z250 group exhibited lower TP and significantly higher microhardness values than the other bulk-fill resin groups before and after thermocycling (P < 0.05). There were no observed differences in the Tetric N-Ceram and Tetric EvoCeram groups before and after thermocycling.
Under the conditions of 10,000 thermal cycles, different curing times did not affect the color change and hardness values of the bulk-fill materials. However, differences were observed among the composite materials. After thermocycling, the surface hardness and TP values decreased in all the resin composites. Depending on the material content, effective results can be obtained from the 20 s polymerization of bulk-fill resin composites.
聚合在光固化树脂复合材料的光学和机械性能中起着重要作用。
本研究旨在评估不同聚合时间对热循环后树脂复合材料颜色变化、透光率参数(TP)和表面硬度的影响。
使用微混合树脂复合材料(Filtek Z250;对照组)和块状填充树脂复合材料(Filtek One Bulk-Fill 修复体、Tetric EvoCeram 块状填充体和 Tetric N-Ceram 块状填充体)。每个块状填充复合材料均单层放置。第一组中块状填充复合材料的聚合在 20 秒内完成,第二组中在 40 秒内完成(n = 10)。Filtek Z250 的聚合完成 2mm(20 秒)+2mm(20 秒)。使用 CIEDE2000 公式计算颜色变化(ΔE)和透光率参数(TP)。热循环前后测量 TP 和表面硬度值。使用单因素和双因素方差分析、配对样本 t 检验和 Tukey 检验(P < 0.05)分析数据。
热循环后,树脂复合材料样品的 ΔE 值为 1.66-2.56。与对照组相比,Filtek One Bulk-Fill 20s 组的颜色变化值最低。Filtek Z250 组在热循环前后的 TP 和显微硬度值均低于其他块状填充树脂组(P < 0.05)。热循环前后 Tetric N-Ceram 和 Tetric EvoCeram 组之间没有观察到差异。
在 10000 次热循环条件下,不同的固化时间不会影响块状填充材料的颜色变化和硬度值。然而,不同的复合材料之间存在差异。热循环后,所有树脂复合材料的表面硬度和 TP 值均降低。根据材料含量,块状填充树脂复合材料 20 秒聚合可获得有效效果。