Suppr超能文献

利用芭蕉和路易波士提取物绿色合成氧化锌纳米颗粒。

A green synthesis of zinc oxide nanoparticles using Musa Paradisiaca and Rooibos extracts.

作者信息

Lyimo G V, Ajayi R F, Maboza E, Adam R Z

机构信息

Restorative Dentistry Department, Faculty of Dentistry, University of the Western Cape, Francie van Zijl Dr, Parow, 7505.

Chemistry Department, Chemical Sciences Building, Faculty of Natural Sciences, University of the Western Cape, Robert Sobukwe Road, Bellville, 7535.

出版信息

MethodsX. 2022 Oct 27;9:101892. doi: 10.1016/j.mex.2022.101892. eCollection 2022.

Abstract

This study describes the single pot synthesis of zinc oxide nanoparticles (ZnO NPs) using a mixture of and for use against the fungi . These nanoparticles are known to be one of the most multifunctional inorganic nanoparticles with effective antifungal and antibacterial activity. The synthesized ZnONPs were characterized by a peak at 290 nm in the UV-vis spectrum while HRSEM confirmed rod-shaped nanoparticles. The FTIR data clearly revealed that the extracts contained -OH  functional groups whose role was capping agents during the nanoparticle synthesis. This study also found that the purity of the green synthesised ZnO NPs (GZnO NPs) was 94.4 %, 91.5 %, and 82.1 %, respectively, using XRD, HRTEM, and HRSEM-EDS. The antifungal activity of ZnONPs was tested against using the Kirby Bauer method. The maximum inhibition zone observed in the ZnO NPs against was confirmed to be 24 mm, a clear indication that the synthesized ZnO NPs have great potential to act as effective antifungal agents.•Zinc nitrate hexahydrate [Zn(NO)·6HO] was used as the inorganic metal oxide precursor.•Extracts of banana () peel and tea leaves of Rooibos ( infused with Buchu () were the organic constituents used as reducing and capping agents during GZnO NPs synthesis.•Validation of the formed GZnO NPs was done using; Ultraviolet-visible spectroscopy (UV-Vis), X-ray spectroscopy (XRD), Fourier-transform Infrared Spectroscopy (FTIR), High-resolution Transmission Electron Microscopy (HRTEM) and Selected Area Electron Diffraction (SAED), and High-Resolution Scanning Electron Microscopy with Energy-Dispersive Spectroscopy (HRSEM-EDS).

摘要

本研究描述了使用[具体物质1]和[具体物质2]的混合物通过单锅法合成氧化锌纳米颗粒(ZnO NPs),用于对抗真菌[真菌名称]。这些纳米颗粒是已知的最具多功能性的无机纳米颗粒之一,具有有效的抗真菌和抗菌活性。合成的ZnONPs在紫外可见光谱中290 nm处有一个峰,而高分辨率扫描电子显微镜(HRSEM)证实为棒状纳米颗粒。傅里叶变换红外光谱(FTIR)数据清楚地表明,提取物含有-OH官能团,其在纳米颗粒合成过程中起封端剂的作用。本研究还发现,使用X射线衍射(XRD)、高分辨率透射电子显微镜(HRTEM)和高分辨率扫描电子显微镜-能谱分析(HRSEM-EDS),绿色合成的ZnO NPs(GZnO NPs)的纯度分别为94.4%、91.5%和82.1%。使用 Kirby Bauer 方法测试了ZnONPs对[真菌名称]的抗真菌活性。在ZnO NPs对[真菌名称]中观察到的最大抑菌圈被确认为24 mm,这清楚地表明合成的ZnONPs有很大潜力作为有效的抗真菌剂。

• 六水合硝酸锌[Zn(NO₃)₂·6H₂O]用作无机金属氧化物前驱体。

• 香蕉([香蕉学名])皮提取物和南非红叶茶([南非红叶茶学名])与布枯([布枯学名])混合浸泡的茶叶是在GZnO NPs合成过程中用作还原剂和封端剂的有机成分。

• 使用紫外可见光谱(UV-Vis)、X射线光谱(XRD)、傅里叶变换红外光谱(FTIR)、高分辨率透射电子显微镜(HRTEM)和选区电子衍射(SAED)以及带能谱分析的高分辨率扫描电子显微镜(HRSEM-EDS)对形成的GZnO NPs进行验证。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2be0/9637953/cf37fd5769f1/ga1.jpg

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验