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新型 CAD/CAM 树脂复合材料的断裂韧性和脆性。

Fracture toughness and brittleness of novel CAD/CAM resin composite block.

机构信息

Glidewell Dental, Irvine, CA, USA.

Glidewell Dental, Irvine, CA, USA.

出版信息

Dent Mater. 2022 Dec;38(12):e308-e317. doi: 10.1016/j.dental.2022.11.012. Epub 2022 Nov 23.

Abstract

OBJECTIVES

To evaluate the fracture toughness and brittleness of a newly developed CAD/CAM resin composite block and compare it with five other resin composite blocks and one polymer-infiltrated ceramic block.

METHODS

Fracture toughness was determined through single-edge notched beam (SENB) method according to ASTM D5045-14. Parallelepiped specimens (thickness × width × length = 1.8 × 3.6 × ∼18 mm) with a V notch (length = ∼1.8 mm) (n = 10) were made from block materials using a low-speed water-cooled diamond precision saw and razor blade. Brittleness index (BI) was calculated from Vickers hardness and fracture toughness. Data were analyzed using one-way ANOVA and post-hoc Tukey tests (p ≤ 0.05).

RESULTS

The experimental block showed significantly higher fracture toughness than all commercial block materials (p < 0.001) and has a brittleness index similar to most commercial blocks (p > 0.05) which have significantly lower brittleness index than Vita Enamic (p < 0.001). A moderate or strong correlation was observed between fracture toughness and flexural strength (Pearson's correlation coefficient R = 0.66) or diametral tensile strength (R = 0.86) or filler loading (R = 0.66), and between brittleness and Vickers hardness (R = 0.87).

SIGNIFICANCE

The new composite block exhibited significantly higher fracture toughness and lower brittleness among the commercial CAD/CAM composite block materials tested, indicating a lower tendency to fracture and marginal chipping, and better machinability. The new composite block with higher fracture toughness and lower brittleness is suitable to use in the fabrication of CAD/CAM indirect restorations with potential long-term clinical success.

摘要

目的

评估一种新型 CAD/CAM 树脂复合材料的断裂韧性和脆性,并与其他五种树脂复合材料和一种聚合物渗透陶瓷进行比较。

方法

根据 ASTM D5045-14 采用单边切口梁(SENB)法测定断裂韧性。使用低速水冷金刚石精密切割锯和剃须刀片从块状材料中制成具有 V 型切口(长度≈1.8mm)(n=10)的棱柱体试样(厚度×宽度×长度=1.8×3.6×≈18mm)。脆性指数(BI)由维氏硬度和断裂韧性计算得出。采用单因素方差分析和事后 Tukey 检验(p≤0.05)对数据进行分析。

结果

实验块的断裂韧性明显高于所有商用块材料(p<0.001),脆性指数与大多数商用块(p>0.05)相似,而明显低于 Vita Enamic(p<0.001)。断裂韧性与弯曲强度(Pearson 相关系数 R=0.66)或直径拉伸强度(R=0.86)或填料加载(R=0.66)之间或脆性与维氏硬度(R=0.87)之间存在中度或强相关性。

意义

在测试的商用 CAD/CAM 复合材料中,新型复合材料具有显著较高的断裂韧性和较低的脆性,表明其断裂和边缘崩裂的倾向较低,可加工性更好。具有较高断裂韧性和较低脆性的新型复合材料适用于 CAD/CAM 间接修复体的制作,具有潜在的长期临床成功。

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