Chen Cai, Han Dongsheng, Wang Mingchuan, Cai Ting, Liang Ningning, Beausir Benoit, Liu Huan, Yang Sen
Sino-French Engineer School, Nanjing University of Science and Technology, Xiaolingwei 200, Nanjing 210094, China.
School of Materials Science and Engineering, Nanjing University of Science and Technology, Xiaolingwei 200, Nanjing 210094, China.
Materials (Basel). 2022 Dec 16;15(24):9005. doi: 10.3390/ma15249005.
In this study, the effect of rotary-die equal-channel angular pressing (RD-ECAP) on the microstructure and texture evolution of GW103 alloy is studied. RD-ECAP processes were carried out for 1, 4 and 12 passes at 450 °C. The mechanical properties and friction behavior of RD-ECAP-processed Mg-10Gd-3Y (wt%) alloy (GW103) are discussed. The results reveal that the size of dynamic recrystallized grains and second-phase particles are significantly refined to about 1.3 μm and 1 μm, respectively. The texture evolution of the processed samples is studied by X-ray diffraction and electron backscattered diffraction techniques. The multiple texture components formed are not observed after the conventional ECAP process. Moreover, different dynamic recrystallization (DRX) mechanisms are systemically analyzed and discussed in view of the texture evolution of ECAP processed samples. The final textures obtained after 12 passes are identified as two types: The C-texture type induced by continuous and discontinuous DRX, and the random texture components induced by reorientation of the initial <101¯0> fiber. Based on the grain refinement, precipitate strengthening and texture weakening mechanisms, a high-performance ternary alloy of Mg-Gd-Y was firstly obtained through 12 passes RD-ECAP processing, with a combination of high yield strength of 312 MPa and a high ductility of 22%. In addition, the friction behaviors are also studied. The multi-pass-processed samples exhibit a relatively lower friction coefficient under a load of 10 N at room temperature.
在本研究中,研究了旋转模等通道转角挤压(RD-ECAP)对GW103合金微观结构和织构演变的影响。在450℃下进行了1道次、4道次和12道次的RD-ECAP工艺。讨论了经RD-ECAP处理的Mg-10Gd-3Y(wt%)合金(GW103)的力学性能和摩擦行为。结果表明,动态再结晶晶粒和第二相粒子的尺寸分别显著细化至约1.3μm和1μm。通过X射线衍射和电子背散射衍射技术研究了加工样品的织构演变。在传统的等通道转角挤压工艺后未观察到形成的多种织构组分。此外,鉴于等通道转角挤压加工样品的织构演变,系统地分析和讨论了不同的动态再结晶(DRX)机制。12道次后获得的最终织构被确定为两种类型:由连续和不连续动态再结晶诱导的C织构类型,以及由初始<101¯0>纤维重新取向诱导的随机织构组分。基于晶粒细化、析出强化和织构弱化机制,通过12道次的RD-ECAP加工首次获得了高性能的Mg-Gd-Y三元合金,其屈服强度高达312MPa,伸长率高达22%。此外,还研究了摩擦行为。多道次加工的样品在室温下10N载荷下表现出相对较低的摩擦系数。