Ahmed Abdulmalek, Adjei Stephen, Elkatatny Salaheldin
College of Petroleum Engineering and Geosciences, King Fahd University of Petroleum & Minerals, 31261 Dhahran, Saudi Arabia.
Department of Petroleum Engineering, Kwame Nkrumah University of Science and Technology, Kumasi 5028, Ghana.
ACS Omega. 2023 Jan 14;8(4):3882-3888. doi: 10.1021/acsomega.2c06289. eCollection 2023 Jan 31.
Heavyweight oil-well cement systems are designed for isolating intervals and supporting the casing at deeper depths where high temperatures and pressures are encountered. The cement slurry should have adequate rheology to ensure efficient placement. Additionally, the hardened cement sheath should be homogeneous with lower porosity and permeability, higher strength, and sufficient flexibility. The effect of vermiculite on hematite-based cement samples has been investigated. The methodology and testing were based on the American Petroleum Institute standards and other recognized recommendations. Fluid properties were characterized by their rheology, while petrophysical and mechanical properties were used to analyze the properties of hardened cement specimens. The vermiculite was used in concentrations of 0.25, 0.5, 1, and 2% by weight of cement (BWOC). The slurries were cured at 3000 psi and 292 °F in cubic and cylindrical molds for 24 h. The results indicate that using 1% BWOC of vermiculite yields the best cement properties. It minimizes the settling of hematite particles to a very low value compared to the base cement as shown by the method of density variation and confirmed by nuclear magnetic resonance. Compared to the base cement slurry, the slurry of 1% BWOC of vermiculite has desirable rheology in terms of plastic viscosity and gel strength. The incorporation of 1% BWOC improves the strength of the cement sheath by 50.7% for the compressive strength and 65% for the tensile strength. Adding 1% vermiculite reduces the permeability and porosity of the cement by 45.8 and 43.5% compared to the control cement. In addition, the 0.7% vermiculite cement is more flexible than the control cement in terms of the elastic properties represented by lower Young's modulus (a reduction of 33%) and higher Poisson's ratio (an increase of 2%).
重量级油井水泥体系旨在隔离井段,并在遇到高温高压的较深深度支撑套管。水泥浆应具有足够的流变性能,以确保有效注入。此外,硬化后的水泥环应均匀,具有较低的孔隙率和渗透率、较高的强度以及足够的柔韧性。已对蛭石对赤铁矿基水泥样品的影响进行了研究。该方法和测试基于美国石油学会标准及其他公认的建议。通过流变性能表征流体性质,而岩石物理和力学性能则用于分析硬化水泥试件的性能。蛭石的用量为水泥重量的0.25%、0.5%、1%和2%。将浆液在3000 psi和292°F的条件下,在立方和圆柱模具中养护24小时。结果表明,使用1%水泥重量的蛭石可获得最佳的水泥性能。与基础水泥相比,通过密度变化法显示并经核磁共振证实,它可将赤铁矿颗粒的沉降最小化至非常低的值。与基础水泥浆相比,1%水泥重量的蛭石浆液在塑性粘度和胶凝强度方面具有理想的流变性能。掺入1%水泥重量的蛭石可使水泥环的抗压强度提高50.7%,抗拉强度提高65%。与对照水泥相比,添加1%蛭石可使水泥的渗透率和孔隙率分别降低45.8%和43.5%。此外,就以较低杨氏模量(降低33%)和较高泊松比(增加2%)表示的弹性性能而言,0.7%蛭石水泥比对照水泥更具柔韧性。